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一种基于理想气体定律的简易毛细管粘度计。

A simple capillary viscometer based on the ideal gas law.

作者信息

Phu Pham Le Hoang, Bautista Luis, Vargas Deyvid C, Luo Xiaolong

机构信息

Department of Mechanical Engineering, The Catholic University of America Washington D.C. 20064 USA

出版信息

RSC Adv. 2018 Aug 29;8(53):30441-30447. doi: 10.1039/c8ra06006a. eCollection 2018 Aug 24.

Abstract

We report a simple, inexpensive and user-friendly capillary viscometer based on the measurement of pressure drop in capillary tubing using the principle of ideal gas law. Viscosity is an important physical property of a fluid that provides molecular information of the fluid's behavior under flow conditions. Measuring viscosity, however, generally requires relatively large fluid volume samples and is expensive with commercial viscometers. Microfluidic viscometers at different levels of complexity can measure fluids at different flow rates with a small sample volume but the cost of commercially available microfluidic viscometers is still high. The reported capillary viscometer is cost-effective, uses small amounts of sample fluid and can measure viscosity under various shear rates. According to the Hagen-Poiseuille equation, the pressure drop of laminar flows in a capillary at a given flow rate is proportional to the viscosity of the fluid. When an enclosed air volume is connected to the upstream of the capillary, the pressure drop can be calculated with the change of the connected air volume, which is reflected by the displacement change of the air-liquid interface in the connecting capillary to the enclosed air volume. Based on these principles, the viscometer was assembled with readily accessible materials, and required no internal sensors or extensive programming. Measurements were successfully performed for five liquids including water, acetone, 2% fat milk, glycerin 30% and glycerin 40%. Except for acetone, the difference between measured and known viscosity was within 4% and highly consistent, well within the 13% uncertainty errors of readily accessible laboratory materials. Overall, the simple viscometer was easily assembled with low cost materials, was portable and accurate, and provided an alternative to expensive commercial viscometers. Finally, the simple capillary viscometer was a good outreach project for K-12 students to understand fluid behavior.

摘要

我们报告了一种基于理想气体定律原理测量毛细管压力降的简单、廉价且用户友好的毛细管粘度计。粘度是流体的一项重要物理性质,它提供了流体在流动条件下行为的分子信息。然而,测量粘度通常需要相对大量的流体样本,并且使用商业粘度计成本高昂。不同复杂程度的微流体粘度计可以在小样本体积下测量不同流速的流体,但市售微流体粘度计的成本仍然很高。所报道的毛细管粘度计具有成本效益,使用少量样本流体,并且可以在各种剪切速率下测量粘度。根据哈根 - 泊肃叶方程,在给定流速下毛细管中层流的压力降与流体的粘度成正比。当一个封闭的空气体积连接到毛细管的上游时,可以通过连接空气体积的变化来计算压力降,这通过连接毛细管中空气 - 液体界面相对于封闭空气体积的位移变化来反映。基于这些原理,该粘度计用容易获得的材料组装而成,不需要内部传感器或大量编程。成功地对包括水、丙酮、2% 脂肪乳、30% 甘油和 40% 甘油在内的五种液体进行了测量。除丙酮外,测量粘度与已知粘度之间的差异在 4% 以内,高度一致,完全在容易获得的实验室材料的 13% 不确定度误差范围内。总体而言,这种简单的粘度计易于用低成本材料组装,便于携带且准确,为昂贵的商业粘度计提供了一种替代方案。最后,这种简单的毛细管粘度计是一个让 K - 12 学生了解流体行为的良好科普项目。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/478f/9085397/aa984a8d7465/c8ra06006a-f1.jpg

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