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漂白剂对经受加速人工老化的复合材料的颜色稳定性、表面粗糙度和显微硬度的作用。

Bleaching agent action on color stability, surface roughness and microhardness of composites submitted to accelerated artificial aging.

作者信息

Rattacaso Raphael Mendes Bezerra, da Fonseca Roberti Garcia Lucas, Aguilar Fabiano Gamero, Consani Simonides, de Carvalho Panzeri Pires-de-Souza Fernanda

机构信息

Graduate Student, Department of Dental Materials and Prosthodontics, Dental School of Ribeirão Preto, University of São Paulo, Ribeirão Preto, SP, Brazil.

出版信息

Eur J Dent. 2011 Apr;5(2):143-9.

Abstract

OBJECTIVES

The purpose of this study was to evaluate the bleaching agent action on color stability, surface roughness and microhardness of composites (Charisma, Filtek Supreme and Heliomolar - A2) submitted to accelerated artificial aging (AAA).

METHODS

A Teflon matrix (12 x 2 mm) was used to fabricate 18 specimens (n=6) which, after polishing (Sof-Lex), were submitted to initial color reading (ΔE), Knoop microhardness (KHN) (50 g/15 s load) and roughness (R(a)) (cut-off 0.25 mm) tests. Afterwards, the samples were submitted to AAA for 384 hours and new color, microhardness and roughness readings were performed. After this, the samples were submitted to daily application (4 weeks) of 16% Carbamide Peroxide (NiteWhite ACP) for 8 hours and kept in artificial saliva for 16 hours. New color, microhardness and roughness readings were made at the end of the cycle, and 15 days after bleaching.

RESULTS

Comparison of the ΔE means (2-way ANOVA, Bonferroni, P<.05) indicated clinically unacceptable color alteration for all composites after AAA, but without significant difference. Statistically significant increase in the KHN values after AAA was observed, but without significant alterations 15 days after bleaching. For R(a) there was no statistically significant difference after AAA and 15 days after bleaching.

CONCLUSIONS

The alterations promoted by the bleaching agent and AAA are material dependent.

摘要

目的

本研究旨在评估漂白剂对经过加速人工老化(AAA)的复合材料(卡瑞斯玛、3M Filtek Supreme和贺利氏 - A2)颜色稳定性、表面粗糙度和显微硬度的作用。

方法

使用聚四氟乙烯基质(12×2毫米)制作18个样本(n = 6),样本在抛光(Sof-Lex)后进行初始颜色读数(ΔE)、努氏显微硬度(KHN)(50克/15秒载荷)和粗糙度(R(a))(截止值0.25毫米)测试。之后,样本进行384小时的AAA处理,并进行新的颜色、显微硬度和粗糙度读数。在此之后,样本每天应用16%过氧化脲(NiteWhite ACP)8小时,持续4周,并在人工唾液中保存16小时。在周期结束时和漂白后15天进行新的颜色、显微硬度和粗糙度读数。

结果

ΔE均值比较(双向方差分析,Bonferroni法,P<0.05)表明,所有复合材料在AAA处理后颜色变化在临床上均不可接受,但无显著差异。观察到AAA处理后KHN值有统计学显著增加,但漂白后15天无显著变化。对于R(a),AAA处理后和漂白后15天无统计学显著差异。

结论

漂白剂和AAA引起的变化取决于材料。

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