Gowda B Thimme, Foro Sabine, Rodrigues Vinola Z, Spandana H S, Fuess Hartmut
Acta Crystallogr Sect E Struct Rep Online. 2011 Feb 12;67(Pt 3):o609. doi: 10.1107/S1600536811004612.
There are two half-mol-ecules in the asymmetric unit of the title compound, C(32)H(30)Cl(4)N(4), in both of which the N-H bonds are syn to the meta-chloro substituents in the adjacent benzene ring. The other two Cl atoms of these two mol-ecules are disordered with occunpancy ratios of 0.79 (2):0.21 (2) and 0.68 (1):0.32 (1). Adjacent chloro-phenyl rings make dihedral angles of 74.3 (2) and 63.0 (2)° in the two mol-ecules. In the crystal, inter-molecular N-H⋯N hydrogen bonds link the mol-ecules into infinite chains.
标题化合物C(32)H(30)Cl(4)N(4)的不对称单元中有两个半分子，在这两个半分子中，N-H键均与相邻苯环上的间位氯取代基呈顺式。这两个分子的另外两个Cl原子无序，占有率分别为0.79 (2):0.21 (2)和0.68 (1):0.32 (1)。在这两个分子中，相邻的氯苯环形成的二面角分别为74.3 (2)°和63.0 (2)°。在晶体中，分子间的N-H⋯N氢键将分子连接成无限长链。
