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1-氯甲基-1,4-重氮双环-[2.2.2]辛烷双（六氟磷酸盐）

1-Chloro-methyl-1,4-diazo-niabicyclo-[2.2.2]octane bis-(hexa-fluoro-phosphate).

作者信息

Zhu Run-Qiang

机构信息

Ordered Matter Science Research Center, College of Chemistry and Chemical Engineering, Southeast University, Nanjing 211189, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 12;67(Pt 2):o346. doi: 10.1107/S1600536811000390.

DOI:10.1107/S1600536811000390
PMID:21523027
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3051799/
Abstract

In the crystal structure of the title compound, C(7)H(15)ClN(2) (2+)·2PF(6) (-), the cations and anions are linked by inter-molecular N-H⋯F hydrogen bonds.

摘要

在标题化合物C(7)H(15)ClN(2)(2+)·2PF(6)(-)的晶体结构中，阳离子和阴离子通过分子间N-H⋯F氢键相连。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7165/3051799/918f664a816f/e-67-0o346-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7165/3051799/f09a9eba7cef/e-67-0o346-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7165/3051799/918f664a816f/e-67-0o346-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7165/3051799/f09a9eba7cef/e-67-0o346-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/7165/3051799/918f664a816f/e-67-0o346-fig2.jpg

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本文引用的文献

1
Discovery of new ferroelectrics: [H2dbco]2 x [Cl3] x [CuCl3(H2O)2] x H2O (dbco = 1,4-Diaza-bicyclo[2.2.2]octane).新型铁电体的发现：[H2dbco]2 x [Cl3] x [CuCl3(H2O)2] x H2O（dbco = 1,4-二氮杂双环[2.2.2]辛烷）。
J Am Chem Soc. 2010 Jun 2;132(21):7300-2. doi: 10.1021/ja102573h.
2
3D framework containing Cu4Br4 cubane as connecting node with strong ferroelectricity.
J Am Chem Soc. 2008 Aug 13;130(32):10468-9. doi: 10.1021/ja803021v. Epub 2008 Jul 18.
3
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
4
Ferroelectric metal-organic framework with a high dielectric constant.具有高介电常数的铁电金属有机框架
J Am Chem Soc. 2006 May 24;128(20):6554-5. doi: 10.1021/ja060856p.