3-氯-N'-(2-氯亚苄基)苯甲酰肼
3-Chloro-N'-(2-chloro-benzyl-idene)benzohydrazide.
作者信息
Lei Yan, Fu Chuan
机构信息
School of Chemistry & Environmental Engineering, Chongqing Three Gorges University, Chongqing 404000, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2011 Jan 15;67(Pt 2):o410. doi: 10.1107/S1600536811001656.
The title compound, C(14)H(10)Cl(2)N(2)O, was prepared from the reaction of 2-chloro-benzaldehyde with 3-chloro-benzo-hydrazide in methanol. The mol-ecule adopts an E configuration about the methyl-idene unit and the two aromatic rings form a dihedral angle of 13.8 (2)°. In the crystal, mol-ecules are linked via inter-molecular N-H⋯O and C-H⋯O hydrogen bonds, forming chains along the c axis.
标题化合物C(14)H(10)Cl(2)N(2)O是由2-氯苯甲醛与3-氯苯甲酰肼在甲醇中反应制备而成。分子围绕亚甲基单元采取E构型，且两个芳香环形成13.8 (2)°的二面角。在晶体中，分子通过分子间N-H⋯O和C-H⋯O氢键相连，沿c轴形成链状结构。
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