Qu Lan-Zhu, Cao Guo-Biao
Department of Chemistry, Ankang University, Ankang Shanxi 725000, People's Republic of China.
Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 27;65(Pt 7):o1705. doi: 10.1107/S160053680902412X.
The title compound, C(14)H(10)BrClN(2)O, was synthesized by the reaction of 2-chloro-benzaldehyde with an equimolar quantity of 3-bromo-benzohydrazide in methanol. The mol-ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 13.0 (2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O hydrogen bonds, forming chains propagating along the c axis.
标题化合物C(14)H(10)BrClN(2)O是由2-氯苯甲醛与等摩尔量的3-溴苯甲酰肼在甲醇中反应合成的。分子中C=N键呈E构型。两个苯环之间的二面角为13.0 (2)°。在晶体结构中,分子通过分子间N-H⋯O氢键相连,形成沿c轴延伸的链。