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{N'-[(E)-(5-溴-2-氧化苯基)(苯基)亚甲基]苯甲酰肼基}吡啶 - 铜(II)

{N'-[(E)-(5-Bromo-2-oxidophen-yl)(phen-yl)methyl-ene]benzohydrazidato}pyridine-copper(II).

作者信息

Zheng Chang-Zheng, Ji Chang-You, Chang Xiu-Li, Zhang Chao-Hua, Xiang Yang-Guang

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Aug 8;65(Pt 9):m1047. doi: 10.1107/S1600536809030463.

DOI:10.1107/S1600536809030463
PMID:21577408
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2970041/
Abstract

The asymmetric unit of title complex, [Cu(C(20)H(13)BrN(2)O(2))(C(5)H(5)N)], contains two independent mol-ecules. In each mol-ecule, the central Cu(II) atom has a square-planar environment formed by the tridentate hydrazone and the monodentate pyridine ligands, with the N atoms in a trans arrangement about the Cu(II) atom.

摘要

标题配合物[Cu(C₂₀H₁₃BrN₂O₂)(C₅H₅N)]的不对称单元包含两个独立的分子。在每个分子中，中心Cu(II)原子具有由三齿腙和单齿吡啶配体形成的平面正方形环境，N原子围绕Cu(II)原子呈反式排列。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5a39/2970041/4c90bd89641c/e-65-m1047-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5a39/2970041/4c90bd89641c/e-65-m1047-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/5a39/2970041/4c90bd89641c/e-65-m1047-fig1.jpg

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本文引用的文献

1
{N'-[(E)-(5-Bromo-2-oxidophen-yl)(phen-yl)methyl-ene]benzohydrazidato}pyridine-nickel(II).{N'-[(E)-(5-溴-2-氧化苯基亚苄基)苯甲基]苯甲酰肼基}吡啶合镍(II)
Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 22;65(Pt 8):m965. doi: 10.1107/S1600536809028207.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.