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聚[水合双(μ(4)-萘-1,4-二羧酸根)(1,10-菲咯啉-5,6-二酮)二锰(II)]

Poly[aqua-bis(μ(4)-naphthalene-1,4-di-carboxyl-ato)(1,10-phenanthroline-5,6-dione)dimanganese(II)].

作者信息

Cong Fang-Di, Yu Feng-Yang, Wei Zhen, Ng Seik Weng

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Nov 7;65(Pt 12):m1543. doi: 10.1107/S1600536809046388.

DOI:10.1107/S1600536809046388
PMID:21578583
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2971822/
Abstract

The three-dimensional coordination polymer, Mn(2)(C(12)H(6)O(4))(2)(C(12)H(6)N(2)O(2))(H(2)O), features a water-coord-inated Mn(II) ion and an N-heterocycle-chelated Mn(II) ion, both in six-coordinate octa-hedral geometries. Of the two rigid dianions, one is bonded to four Mn(II) ions, with each of the O atoms being connected to a different metal ion. The other dianion uses one carboxyl-ate group to chelate to one Mn(II) ion and its other carboxyl-ate group to bind to two Mn(II) ions.

摘要

三维配位聚合物Mn(2)(C(12)H(6)O(4))(2)(C(12)H(6)N(2)O(2))(H(2)O)具有一个水配位的Mn(II)离子和一个N杂环螯合的Mn(II)离子，二者均处于六配位八面体几何构型。在这两个刚性二价阴离子中，一个与四个Mn(II)离子键合，每个O原子与不同的金属离子相连。另一个二价阴离子用一个羧酸根基团螯合一个Mn(II)离子，其另一个羧酸根基团与两个Mn(II)离子结合。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c62c/2971822/7e0bde49f00c/e-65-m1543-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c62c/2971822/7e0bde49f00c/e-65-m1543-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c62c/2971822/7e0bde49f00c/e-65-m1543-fig1.jpg

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本文引用的文献

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Acta Crystallogr Sect E Struct Rep Online. 2009 Mar 25;65(Pt 4):m421. doi: 10.1107/S1600536809009301.
2
catena-Poly[[[bis-[4-(1H-1,3,7,8-tetra-azacyclo-penta-[l]phenanthren-2-yl)phenol-κN,N]manganese(II)]-μ-naphthalene-1,4-dicarboxyl-ato-κO:O] naphthalene-1,4-dicarboxylic acid hemisolvate monohydrate].链状聚[[[双-[4-(1H-1,3,7,8-四氮杂环戊并[a]菲-2-基)苯酚-κN,N]锰(II)]-μ-萘-1,4-二羧酸根-κO:O]萘-1,4-二羧酸半溶剂化物一水合物]
Acta Crystallogr Sect E Struct Rep Online. 2008 Apr 23;64(Pt 5):m701-2. doi: 10.1107/S160053680801074X.
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A short history of SHELX.
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Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.