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本文引用的文献

1
Deacetyl- tenuazonic acid.脱乙酰基细交链孢菌酮酸
Acta Crystallogr Sect E Struct Rep Online. 2009 May 7;65(Pt 6):o1201. doi: 10.1107/S1600536809015372.
2
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Acta Crystallogr Sect E Struct Rep Online. 2008 Mar 5;64(Pt 4):o657. doi: 10.1107/S1600536808005515.
3
Determination of the Alternaria mycotoxin tenuazonic acid in cereals by high-performance liquid chromatography-electrospray ionization ion-trap multistage mass spectrometry after derivatization with 2,4-dinitrophenylhydrazine.用2,4-二硝基苯肼衍生化后，通过高效液相色谱-电喷雾电离离子阱多级质谱法测定谷物中的链格孢霉菌毒素细交链孢菌酮酸。
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A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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Studies in the biochemistry of micro-organisms. 106. Metabolites of Alternaria tenuis auct.: the structure of tenuazonic acid.微生物生物化学研究。106. 细交链孢菌的代谢产物：细交链孢菌酮酸的结构
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去乙酰基细交链孢菌酮酸对甲苯磺酰腙

Deacetyl tenuazonic acid p-toluene-sulfonyl-hydrazone.

作者信息

Siegel David, Blaske Franziska, Koch Matthias, Emmerling Franziska, Nehls Irene

机构信息

BAM Federal Institute for Materials Research and Testing, Abteilung Analytische Chemie; Referenzmaterialien, Richard-Willstätter-Strasse 11, D-12489 Berlin-Adlershof, Germany.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Nov 21;65(Pt 12):o3136. doi: 10.1107/S1600536809048958.

DOI:10.1107/S1600536809048958
PMID:21578857
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2972091/
Abstract

The title compound {systematic name: 4-methyl-N'-[(3E)-2-(1-methyl-prop-yl)-5-oxopyrrolidin-3-yl-idene]benzene-sulfono-hydrazide}, C(15)H(21)N(3)O(3)S, is the condensation product of deacetyl tenuazonic acid (DTA) and p-toluene-sulfonohydrazide. The crystal structure consists of chains along [100] linked by N-H⋯O hydrogen bonds.

摘要

标题化合物{系统名称：4-甲基-N'-[(3E)-2-(1-甲基丙基)-5-氧代吡咯烷-3-亚基]苯磺酰肼}，C₁₅H₂₁N₃O₃S，是脱乙酰基细交链孢菌酮酸（DTA）与对甲苯磺酰肼的缩合产物。晶体结构由沿[100]方向的链组成，通过N-H⋯O氢键相连。