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N'-(5-溴-1H-吲哚-3-基亚甲基)-3,4,5-三羟基苯甲酰肼

N'-(5-Bromo-1H-indol-3-ylmethyl-idene)-3,4,5-trihydroxy-benzohydrazide.

作者信息

Khaledi Hamid, Mohd Ali Hapipah, Ng Seik Weng

机构信息

Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Oct 11;64(Pt 11):o2108. doi: 10.1107/S1600536808031991.

DOI:10.1107/S1600536808031991
PMID:21580972
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2959687/
Abstract

The two aromatic parts of the title mol-ecule, C(16)H(12)BrN(3)O(4), are connected through a conjugated -CH=N-NH-C(O)- fragment to furnish an almost planar mol-ecule. Adjacent mol-ecules are linked by N-H⋯O and O-H⋯O hydrogen bonds into a three-dimensional network. An intramolecular O-H⋯O link also occurs.

摘要

标题分子C(16)H(12)BrN(3)O(4)的两个芳香部分通过一个共轭的-CH=N-NH-C(O)-片段相连，形成一个近乎平面的分子。相邻分子通过N-H⋯O和O-H⋯O氢键连接成三维网络。分子内也存在O-H⋯O连接。

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N'-(5-Bromo-1H-indol-3-ylmethyl-idene)-3,4,5-trihydroxy-benzohydrazide.N'-(5-溴-1H-吲哚-3-基亚甲基)-3,4,5-三羟基苯甲酰肼
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引用本文的文献

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Acta Crystallogr Sect E Struct Rep Online. 2009 Jul 18;65(Pt 8):o1920. doi: 10.1107/S1600536809027032.
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N'-[(5-Chloro-1H-indol-3-yl)methyl-ene]-3,4,5-trihydroxy-benzohydrazide.N'-[(5-氯-1H-吲哚-3-基)亚甲基]-3,4,5-三羟基苯甲酰肼
Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 20;65(Pt 1):o169. doi: 10.1107/S160053680804258X.
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本文引用的文献

1
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
3,4,5-三羟基-N'-(1H-吲哚-3-基亚甲基)苯甲酰肼五水合物
Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 29;64(Pt 12):o2481. doi: 10.1107/S1600536808039342.
4
3,4,5-Trihydr-oxy-N'-(1H-indol-2-ylmethyl-idene)benzohydrazide-1H-indole-2-carbaldehyde azine-methanol (2/1/2).3,4,5-三羟基-N'-(1H-吲哚-2-基亚甲基)苯甲酰肼-1H-吲哚-2-甲醛连氮-甲醇(2/1/2)
Acta Crystallogr Sect E Struct Rep Online. 2009 Dec 12;66(Pt 1):o105-6. doi: 10.1107/S1600536809052465.