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（E）-N'-（5-溴-2-羟基-亚苄基）-对甲苯磺酰肼

(E)-N'-(5-Bromo-2-hydroxy-benzyl-idene)-p-toluene-sulfonohydrazide.

作者信息

Kia Reza, Fun Hoong-Kun, Kargar Hadi

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 13;64(Pt 12):o2341. doi: 10.1107/S1600536808037069.

DOI:10.1107/S1600536808037069
PMID:21581316
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2959853/
Abstract

The title compound, C(14)H(13)BrN(2)O(3)S, features an intra-molecular O-H⋯N hydrogen bond which generates an S(6) ring motif. The dihedral angle between the two benzene rings is 86.47 (6)°. Inter-molecular N-H⋯O and C-H⋯O inter-actions link neighbouring mol-ecules via R(2) (2)(13) ring motifs, forming one-dimensional extended chains along the c axis.

摘要

标题化合物C(14)H(13)BrN(2)O(3)S具有分子内O-H⋯N氢键，形成了一个S(6)环模式。两个苯环之间的二面角为86.47 (6)°。分子间N-H⋯O和C-H⋯O相互作用通过R(2) (2)(13)环模式连接相邻分子，沿c轴形成一维延伸链。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1063/2959853/5dae8b1672ee/e-64-o2341-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1063/2959853/327c358421ce/e-64-o2341-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1063/2959853/5dae8b1672ee/e-64-o2341-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1063/2959853/327c358421ce/e-64-o2341-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1063/2959853/5dae8b1672ee/e-64-o2341-fig2.jpg

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(E)-N'-(4-Chloro-benzyl-idene)-p-toluene-sulfonohydrazide 0.15-hydrate.
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Acta Crystallogr Sect E Struct Rep Online. 2009 Mar 25;65(Pt 4):o821-2. doi: 10.1107/S1600536809009751.
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Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 22;64(Pt 12):o2424. doi: 10.1107/S1600536808038695.