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（E）-N'-（5-溴-2-羟基-亚苄基）-3,4,5-三甲氧基-苯甲酰肼

(E)-N'-(5-Bromo-2-hydroxy-benzyl-idene)-3,4,5-trimethoxy-benzohydrazide.

作者信息

Zhao Zhen-Dong, Wang Yu-Min, Chen Yu-Xiang, Bi Liang-Wu

机构信息

Institute of Chemical Industry of Forest Products, Chinese Academy of Forestry, Nanjing 210042, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 22;64(Pt 12):o2408. doi: 10.1107/S1600536808038464.

DOI:10.1107/S1600536808038464
PMID:21581377
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2960056/
Abstract

The mol-ecule of the title compound, C(17)H(17)BrN(2)O(5), assumes an E configuration, with the 5-bromo-2-hydroxy-phenyl and benzohydrazide units located on opposite sites of the C=N double bond. The dihedral angle between the planes of the two benzene rings is 32.48 (15)°. The crystal structure is stabilized by intra-molecular O-H⋯N and inter-molecular N-H⋯O hydrogen bonds.

摘要

标题化合物C(17)H(17)BrN(2)O(5)的分子呈E构型，5-溴-2-羟基苯基和苯甲酰肼单元位于C=N双键的相对位置。两个苯环平面之间的二面角为32.48 (15)°。晶体结构通过分子内O-H⋯N和分子间N-H⋯O氢键得以稳定。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8612/2960056/53b9fcabae80/e-64-o2408-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8612/2960056/582c695ebd1c/e-64-o2408-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8612/2960056/53b9fcabae80/e-64-o2408-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8612/2960056/582c695ebd1c/e-64-o2408-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8612/2960056/53b9fcabae80/e-64-o2408-fig2.jpg

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本文引用的文献

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Acta Crystallogr Sect E Struct Rep Online. 2008 May 7;64(Pt 6):o1009. doi: 10.1107/S1600536808006077.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.