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N-[4-(β-D-吡喃阿洛糖氧基)亚苄基]甲胺

N-[4-(β-d-Allopyranos-yloxy)benzyl-idene]methyl-amine.

作者信息

Lv Shi-Ming, Zheng Lei, Zhao Hui, Li Ying, Yin Shu-Fan

机构信息

College of Chemistry, Sichuan University, Chengdu 610064, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jan 10;65(Pt 2):o290. doi: 10.1107/S1600536809000944.

DOI:10.1107/S1600536809000944
PMID:21581901
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2968321/
Abstract

The title compound, C(14)H(19)NO(6), was synthesized by the condensation reaction between hecilid (4-formyl-phenl-β-d-allopyran-oside) and methyl-amine in methanol. In the crystal structure, the pyran ring adopts a chair conformation and adjacent mol-ecules are linked by inter-molecular O-H⋯O and O-H⋯N hydrogen bonds, forming a three-dimensional network.

摘要

标题化合物C(14)H(19)NO(6)是通过海西利德（4-甲酰基苯基-β-D-阿洛吡喃糖苷）与甲胺在甲醇中发生缩合反应合成的。在晶体结构中，吡喃环呈椅式构象，相邻分子通过分子间O-H⋯O和O-H⋯N氢键相连，形成三维网络。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/be3c/2968321/17e917487ee7/e-65-0o290-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/be3c/2968321/17e917487ee7/e-65-0o290-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/be3c/2968321/17e917487ee7/e-65-0o290-fig1.jpg

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A short history of SHELX.SHELX简史。
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