Lv Shi-Ming, Zheng Lei, Zhao Hui, Li Ying, Yin Shu-Fan
College of Chemistry, Sichuan University, Chengdu 610064, People's Republic of China.
Acta Crystallogr Sect E Struct Rep Online. 2009 Jan 10;65(Pt 2):o290. doi: 10.1107/S1600536809000944.
The title compound, C(14)H(19)NO(6), was synthesized by the condensation reaction between hecilid (4-formyl-phenl-β-d-allopyran-oside) and methyl-amine in methanol. In the crystal structure, the pyran ring adopts a chair conformation and adjacent mol-ecules are linked by inter-molecular O-H⋯O and O-H⋯N hydrogen bonds, forming a three-dimensional network.
标题化合物C(14)H(19)NO(6)是通过海西利德(4-甲酰基苯基-β-D-阿洛吡喃糖苷)与甲胺在甲醇中发生缩合反应合成的。在晶体结构中,吡喃环呈椅式构象,相邻分子通过分子间O-H⋯O和O-H⋯N氢键相连,形成三维网络。