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4-Ethyl-amino-3-nitro-benzoic acid.

作者信息

Narendra Babu Shivanagere Nagojappa, Abdul Rahim Aisyah Saad, Abd Hamid Shafida, Quah Ching Kheng, Fun Hoong-Kun

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Apr 22;65(Pt 5):o1079. doi: 10.1107/S1600536809014196.

Abstract

In the title compound, C(9)H(10)N(2)O(4), an intra-molecular N-H⋯O hydrogen-bond inter-action generates an S(6) ring motif. The nitro group is slightly twisted away from its attached benzene ring [dihedral angle = 15.29 (15)°]. In the crystal structure, mol-ecules are stacked down the a axis caused by short O⋯O(-1-x, -y, 2-z) contacts of 2.6481 (16) Å involving the O atoms of the nitro groups. The crystal packing is consolidated by inter-molecular O-H⋯O hydrogen bonds, linking the mol-ecules into centrosymmetric dimers.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/2c33/2977758/33773088e39f/e-65-o1079-fig1.jpg

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