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Bis{1-[(E)-o-tolyl-diazen-yl]-2-naphtho-l-ato}copper(II).

作者信息

Tai Wan-Ju, Li Chi-Huan, Li Chen-Yu, Ko Bao-Tsan

机构信息

Department of Chemistry, Chung Yuan Christian University, Chung-Li 320, Taiwan.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 30;66(Pt 10):m1315. doi: 10.1107/S1600536810037888.

DOI:10.1107/S1600536810037888
PMID:21587451
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2983183/
Abstract

In the title complex, [Cu(C(17)H(13)N(2)O)(2)], the Cu(II) atom is tetra-coordinated by two N atoms and two O atoms from two bidentate 1-[(E)-o-tolyl-diazen-yl]-2-naphtho-late ligands, forming a slightly distorted square-planar environment. The two N atoms and two O atoms around the Cu(II) atom are trans to each other, with an O-Cu-O bond angle of 177.00 (9)° and an N-Cu-N bond angle of 165.63 (10)°. The average distances between the Cu(II) atom and the coordinated O and N atoms are 1.905 (2) and 1.995 (2)Å, respectively.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/970c/2983183/e7ec73d6f6a6/e-66-m1315-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/970c/2983183/e83b9e91d630/e-66-m1315-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/970c/2983183/e7ec73d6f6a6/e-66-m1315-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/970c/2983183/e83b9e91d630/e-66-m1315-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/970c/2983183/e7ec73d6f6a6/e-66-m1315-fig2.jpg

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本文引用的文献

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2
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3
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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Chemical fixation of carbon dioxide catalyzed by binaphthyldiamino Zn, Cu, and Co salen-type complexes.
J Org Chem. 2003 Feb 21;68(4):1559-62. doi: 10.1021/jo020191j.