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N'-[(1E)-1-(3,5-二氯-2-羟基苯基)亚丙基]-4-甲氧基苯甲酰肼一水合物

N'-[(1E)-1-(3,5-Dichloro-2-hy-droxy-phen-yl)propyl-idene]-4-meth-oxy-benzohydrazide monohydrate.

作者信息

He Chun-Hong, Zhang Jian-Ping, Chang Jian-Guo

机构信息

Department of Material Science and Chemical Engineering, Taishan University, 271021 Taian, Shandong, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2010 Sep 25;66(Pt 10):o2620. doi: 10.1107/S1600536810037293.

DOI:10.1107/S1600536810037293
PMID:21587594
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2983233/
Abstract

The title compound, C(17)H(16)Cl(2)N(2)O(3)·H(2)O, displays a trans conformation with respect to the C=N double bond. The dihedral angle between the two benzene rings is 30.77 (5)° and there is one intra-molecular N-H⋯O hydrogen bond. In the crystal, mol-ecules are linked by hydrogen bonding to the water molecules of crystallization, which acts as both an acceptor and a donor, into a three-dimensional network.

摘要

标题化合物C(17)H(16)Cl(2)N(2)O(3)·H(2)O关于C=N双键呈反式构象。两个苯环之间的二面角为30.77 (5)°，存在一个分子内N-H⋯O氢键。在晶体中，分子通过氢键与结晶水分子相连，结晶水分子既作为受体又作为供体，形成三维网络。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d26e/2983233/ff96fd8d15bd/e-66-o2620-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d26e/2983233/cac025f85d40/e-66-o2620-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d26e/2983233/ff96fd8d15bd/e-66-o2620-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d26e/2983233/cac025f85d40/e-66-o2620-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d26e/2983233/ff96fd8d15bd/e-66-o2620-fig2.jpg

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