Kumar Raju Suresh, Osman Hasnah, Perumal Subbu, Hemamalini Madhukar, Fun Hoong-Kun
Acta Crystallogr Sect E Struct Rep Online. 2010 Oct 9;66(Pt 11):o2736-7. doi: 10.1107/S1600536810039310.
In the title compound, C(33)H(28)N(2)O(2)·0.25C(2)H(6)O·0.6H(2)O, the piperidone ring adopts a chair conformation and the pyrrolidine ring adopts an envelope conformation. The dihedral angle between the two phenyl rings is 70.83 (16)°. One of the N atoms of the organic mol-ecule is disordered over two positions in a 0.52 (4):0.48 (4) ratio and the two solvent mol-ecules are partially occupied and show high displacement parameters. In the crystal, mol-ecules are connected by inter-molecular O-H⋯O and C-H⋯O hydrogen bonds, forming a three-dimensional network.
在标题化合物C(33)H(28)N(2)O(2)·0.25C(2)H(6)O·0.6H(2)O中，哌啶酮环呈椅式构象，吡咯烷环呈信封式构象。两个苯环之间的二面角为70.83 (16)°。有机分子中的一个N原子在两个位置上无序分布，比例为0.52 (4):0.48 (4)，两个溶剂分子部分占据，且位移参数较高。在晶体中，分子通过分子间的O-H⋯O和C-H⋯O氢键相连，形成三维网络。
