Department of Advanced Prosthodontics, Graduate School of Biomedical Sciences, Hiroshima University, Hiroshima, Japan.
J Prosthodont Res. 2012 Apr;56(2):136-41. doi: 10.1016/j.jpor.2011.05.001. Epub 2011 Jun 12.
The purpose of this study was to determine the durability of the peel bond of commercial resilient denture liners to a denture base resin using a thermal cycling test.
Eight commercial resilient denture liners (five silicone and three acrylic) were used in the study. The samples were exposed to thermal cycles between 5°C and 55°C for 1 min for 0, 1,250, 2,500, 5,000 and 10,000 cycles. The test samples were placed under tension until failure in a materials testing machine using a crosshead speed of 20 mm/min. The modes of debonding were characterized as tear, peel or snap. Statistical analysis was performed using one-way and two-way analysis of variance and Student-Newman-Keuls multiple comparison tests (α=.05).
A significant difference was found between different resilient denture liners for peel bond strength at 0 cycles. No extreme influence on the peel bond strength was observed under any of the thermal cycles. The snap mode of debonding was observed in most samples of all materials for all cycles.
All resilient denture liners tested had a sufficiently strong bond to the denture base resin. Within the limitations of this study, the results show that all of the materials were acceptable for clinical use, having met the accepted adequate bond strength for resilient denture liners of 0.45 MPa.
本研究旨在通过热循环试验确定商用弹性义齿衬垫与义齿基托树脂之间的剥离粘结耐久性。
本研究使用了八种商用弹性义齿衬垫(五种硅橡胶和三种丙烯酸酯)。样本在 5°C 和 55°C 之间经历 1 分钟的热循环,循环次数为 0、1,250、2,500、5,000 和 10,000 次。测试样本在材料试验机中以 20mm/min 的十字头速度置于张力下直至失效。通过撕裂、剥离或断裂的模式来描述脱粘的方式。采用单向和双向方差分析以及学生-纽曼-凯尔斯多重比较检验(α=.05)进行统计分析。
在 0 循环时,不同弹性义齿衬垫之间的剥离粘结强度存在显著差异。在任何热循环下,都没有观察到对剥离粘结强度的极端影响。在所有循环中,大多数材料的样本都观察到了断裂模式的脱粘。
所有测试的弹性义齿衬垫与义齿基托树脂之间都具有足够强的粘结力。在本研究的限制范围内,结果表明所有材料都可临床使用,满足了弹性义齿衬垫 0.45MPa 的可接受的足够粘结强度标准。