Wang Haiyang, Xia Guangxin, Liu Xuejun, Shen Jingkang
Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1437. doi: 10.1107/S1600536811017764. Epub 2011 May 20.
The title compound, C(24)H(30)N(2)O(4), was obtained by the reaction of (2R,6S)-4-(tert-but-oxy-carbon-yl)-6-methyl-morpho-line-2-carb-oxy-lic acid with diphenyl-methanamine in dimethyl-formamide solution. The morpholine ring is in a chair conformation. In the crystal, weak inter-molecular C-H⋯O hydrogen bonds link mol-ecules into chains along the b axis.
标题化合物C(24)H(30)N(2)O(4)是通过(2R,6S)-4-(叔丁氧羰基)-6-甲基吗啉-2-羧酸与二苯甲胺在二甲基甲酰胺溶液中反应得到的。吗啉环呈椅式构象。在晶体中,弱的分子间C-H⋯O氢键将分子沿b轴连接成链。