Faust Rüdiger, Nauroozi Djawed, Bruhn Clemens, Koch Britta, Kuhlich Paul, Piechotta Christian, Nehls Irene
Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1462-3. doi: 10.1107/S1600536811018009. Epub 2011 May 20.
The title compound (AHTN-OH), C(17)H(26)O, was prepared in order to provide standard materials for the qualitative and quanti-tative analysis of environmental pollutants. The mol-ecule possesses a chiral C atom, although the structure determination was performed on racemic material, expressed in the structure as disordered chiral sites. The asymmetric unit consists of four AHTN-OH mol-ecules containing an hy-droxy group and forming a tetra-meric cyclic motif built up by four strong hydrogen bonds between these hy-droxy groups and additionally by two weak C-H⋯π inter-actions. Furthermore, these tetra-mers are linked via very weak C-H⋯π inter-actions, forming chains along the c axis.
制备标题化合物（AHTN-OH，C₁₇H₂₆O）是为了提供用于环境污染物定性和定量分析的标准物质。该分子具有一个手性碳原子，尽管结构测定是在消旋物质上进行的，在结构中表示为无序的手性位点。不对称单元由四个含有羟基的AHTN-OH分子组成，通过这些羟基之间的四个强氢键以及另外两个弱C-H⋯π相互作用形成一个四聚体环状结构。此外，这些四聚体通过非常弱的C-H⋯π相互作用连接，沿c轴形成链状结构。
