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N-(4-Fluoro-benz-yl)-3-nitro-pyridine-2,6-diamine.

作者信息

Ge Ji-Long, Qian Xiao-Min

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1481. doi: 10.1107/S1600536811018642. Epub 2011 May 20.

DOI:10.1107/S1600536811018642
PMID:21754850
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3120364/
Abstract

In the title compound, C(12)H(11)FN(4)O(2), the pyridine ring is connected to a benzene ring by a -CH(2)-NH(2)- chain. The nitro group is twisted out of the pyridine ring plane [torsion angle O-N-C-C = 10.41 (10)°]. An intramolecular N-H⋯O hydrogen bond occurs. The fluoro-benzene ring is disordered over two positions [occupancy ratio = 0.59 (3):0.41 (3)]. Inter-molecular N-H⋯O and N-H⋯N hydrogen bonds stabilize the crystal structure.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/573a/3120364/0a4bf678e50a/e-67-o1481-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/573a/3120364/9409ac0a86e5/e-67-o1481-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/573a/3120364/0a4bf678e50a/e-67-o1481-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/573a/3120364/9409ac0a86e5/e-67-o1481-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/573a/3120364/0a4bf678e50a/e-67-o1481-fig2.jpg

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