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4-氯-N-(2,5-二甲基苯基)苯磺酰胺

4-Chloro-N-(2,5-dimethyl-phen-yl)benzene-sulfonamide.

作者信息

Shakuntala K, Foro Sabine, Gowda B Thimme

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Jun 1;67(Pt 6):o1541. doi: 10.1107/S1600536811019660. Epub 2011 May 28.

DOI:10.1107/S1600536811019660
PMID:21754900
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3120369/
Abstract

The title compound, C(14)H(14)ClNO(2)S, contains two molecules in the asymmetric unit with different conformations. The C-SO(2)-NH-C torsion angles are 65.3 (2) and 54.6 (2)° and the aromatic rings are tilted relative to each other by 59.3 (1) and 45.8 (1)° in the two mol-ecules. In the crystal, inversion symmetry results in dimers linked by pairs of N-H⋯O hydrogen bonds for both molecules.

摘要

标题化合物C(14)H(14)ClNO(2)S的不对称单元中包含两个构象不同的分子。两个分子中C-SO(2)-NH-C扭转角分别为65.3 (2)°和54.6 (2)°，芳环彼此倾斜角度分别为59.3 (1)°和45.8 (1)°。在晶体中，两个分子均通过N-H⋯O氢键对形成的二聚体，这是由反演对称性导致的。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e09/3120369/fea10ac7350a/e-67-o1541-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e09/3120369/396e680b252f/e-67-o1541-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e09/3120369/fea10ac7350a/e-67-o1541-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e09/3120369/396e680b252f/e-67-o1541-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e09/3120369/fea10ac7350a/e-67-o1541-fig2.jpg

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N-(2,5-Dimethyl-phen-yl)benzene-sulfonamide.N-（2,5-二甲基-苯基）苯磺酰胺
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Acta Crystallogr D Biol Crystallogr. 2009 Feb;65(Pt 2):148-55. doi: 10.1107/S090744490804362X. Epub 2009 Jan 20.
5
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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Hydrogen bonding in sulfonamides.磺酰胺中的氢键。
J Pharm Sci. 2001 Dec;90(12):2058-77. doi: 10.1002/jps.1157.