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Bis{μ-1,3-bis-[(2-methyl-1H-benzimid-azol-1-yl)meth-yl]benzene-κN:N}bis-(diiodidocadmium).

作者信息

Hu Jiyong, Liu Junhong, Zhao Jin'an

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2011 Nov;67(Pt 11):m1566. doi: 10.1107/S1600536811042334. Epub 2011 Oct 22.

DOI:10.1107/S1600536811042334
PMID:22219804
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3246984/
Abstract

In the title compound, [Cd(2)I(4)(C(24)H(22)N(4))(2)], the 1,3-bis-[(2-methyl-1H-benzimidazol-1-yl)meth-yl]benzene ligand bridges two CdI(2) units, forming a centrosymmetric dinuclear complex. The Cd(II) atom adopts a distorted tetra-hedral coordination geometry. In the crystal, complex mol-ecules are linked into columns parallel to [101] by π-π stacking inter-actions, with centroid-centroid distances of 3.558 (2) Å.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/da5d/3246984/016d3a98b171/e-67-m1566-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/da5d/3246984/016d3a98b171/e-67-m1566-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/da5d/3246984/016d3a98b171/e-67-m1566-fig1.jpg

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本文引用的文献

1
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Acta Crystallogr Sect E Struct Rep Online. 2009 May 7;65(Pt 6):m613. doi: 10.1107/S1600536809015943.
2
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Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
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Crucial role of the counteranion on the templation of metallomacrocycles and a 3D network: synthesis, characterization, and structural analysis.抗衡阴离子在金属大环化合物和三维网络模板化过程中的关键作用：合成、表征及结构分析
Inorg Chem. 2003 Sep 8;42(18):5654-9. doi: 10.1021/ic0340884.