Morishita Kohei, Hayashi Kouichi, Nakajima Kazuo
Department of Socio-Environmental Energy Science, Kyoto University, Yoshida-Honmachi, Sakyo-ku, Kyoto, Japan.
Rev Sci Instrum. 2012 Jan;83(1):013112. doi: 10.1063/1.3677326.
Time-resolved x-ray spectrometry using an ultrastrong x-ray source such as an x-ray free electron laser is one of the new trends in the field of x-ray physics. To achieve such time-resolved measurement, the development of an one-shot spectrometer with a wide wavelength range, high efficiency, and good energy resolution is an essential prerequisite. Here we developed an integrated conical Ge crystal analyzer consisting of several conical rings, which were connected using spline surfaces to form a single body using our previously developed hot deformation technique, which can form a Si or Ge wafer into an arbitrary and accurate shape. We simultaneously focused several characteristic lines from an alloy sample onto different positions on a small x-ray charge-coupled device with very high image brightness (gain relative to planar analyzer: 100) and a good spatial resolution of 9-13 eV. The small radius of curvature of the crystal (28-50 mm) enabled us to realize a very short sample-detector distance of 214.4 mm. The present result shows the possibility of realizing a new focusing x-ray crystal spectrograph that can control the focal position as desired.
使用诸如X射线自由电子激光等超强X射线源的时间分辨X射线光谱学是X射线物理学领域的新趋势之一。为了实现这种时间分辨测量,开发一种具有宽波长范围、高效率和良好能量分辨率的单次光谱仪是必不可少的先决条件。在这里,我们开发了一种集成锥形锗晶体分析仪,它由几个锥形环组成,这些锥形环使用样条曲面连接,利用我们先前开发的热变形技术形成一个整体,该技术可以将硅或锗晶片加工成任意精确的形状。我们同时将来自合金样品的几条特征线聚焦到一个小型X射线电荷耦合器件上的不同位置,该器件具有非常高的图像亮度(相对于平面分析仪的增益:100)和9 - 13 eV的良好空间分辨率。晶体的小曲率半径(28 - 50毫米)使我们能够实现214.4毫米的极短样品 - 探测器距离。目前的结果表明,有可能实现一种新型的聚焦X射线晶体光谱仪,它可以根据需要控制焦点位置。