Faculty of Technology and Metallurgy, University of Belgrade, Karnegijeva 4, 11120 Belgrade, Serbia.
Sensors (Basel). 2010;10(1):901-12. doi: 10.3390/s100100901. Epub 2010 Jan 25.
The subject of this study is the development of flavor wax formulations aimed for food and feed products. The melt dispersion technique was applied for the encapsulation of ethyl vanillin in wax microcapsules. The surface morphology of microparticles was investigated using scanning electron microscope (SEM), while the loading content was determined by HPLC measurements. This study shows that the decomposition process under heating proceeds in several steps: vanilla evaporation occurs at around 200 °C, while matrix degradation starts at 250 °C and progresses with maxima at around 360, 440 and 520 °C. The results indicate that carnauba wax is an attractive material for use as a matrix for encapsulation of flavours in order to improve their functionality and stability in products.
本研究的主题是开发用于食品和饲料产品的风味蜡制剂。采用熔融分散技术将乙基香兰素包封在蜡微胶囊中。使用扫描电子显微镜(SEM)研究了微粒的表面形态,而通过高效液相色谱(HPLC)测量确定了载药量。本研究表明,加热下的分解过程分为几个步骤:香草蒸发发生在 200°C 左右,而基质降解在 250°C 开始,并在 360、440 和 520°C 左右达到最大值。结果表明,巴西棕榈蜡是一种有吸引力的材料,可用作包封香料的基质,以提高其在产品中的功能和稳定性。