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本文引用的文献

1
[Bis(diphenyl-phosphan-yl)dimethyl-silane-κP,P']tetra-carbonyl-chromium(0).[双（二苯基膦基）二甲基硅烷-κP,P']四羰基铬(0)
Acta Crystallogr Sect E Struct Rep Online. 2010 Oct 31;66(Pt 11):m1494. doi: 10.1107/S1600536810043679.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
3
Synthesis of macrocyclic aluminum-phosphorus and gallium-phosphorus compounds.
Angew Chem Int Ed Engl. 2006 Mar 27;45(14):2302-5. doi: 10.1002/anie.200503531.

四羰基[双（二苯基膦基）四甲基二硅氧烷-κP，P']铬(0)

Tetra-carbon-yl[bis-(diphenyl-phosphan-yl)tetra-methyl-disiloxane-κP,P']chromium(0).

作者信息

Peulecke Normen, Müller Bernd H, Spannenberg Anke, Rosenthal Uwe

机构信息

Leibniz-Institut für Katalyse e. V. an der Universität Rostock, Albert-Einstein-Strasse 29a, 18059 Rostock, Germany.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Feb 1;68(Pt 2):m119. doi: 10.1107/S1600536812000219. Epub 2012 Jan 7.

DOI:10.1107/S1600536812000219
PMID:22346807
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3274860/
Abstract

The title compound, [Cr(C(28)H(32)OP(2)Si(2))(CO)(4)], was obtained by the ligand-exchange reaction of Cr(CO)(6) with (Ph(2)PSiMe(2))(2)O in refluxing toluene. The CrC(4)P(2) coordination geometry is distorted octa-hedral, with a P-Cr-P bite angle of 99.22 (4)°.

摘要

标题化合物[Cr(C₂₈H₃₂OP₂Si₂)(CO)₄]是通过Cr(CO)₆与(Ph₂PSiMe₂)₂O在回流甲苯中进行配体交换反应制得的。CrC₄P₂的配位几何形状为扭曲的八面体，P-Cr-P夹角为99.22 (4)°。