Institute of Nano Science and Nano Technology, University of Kashan, Kashan, Islamic Republic of Iran.
Ultrason Sonochem. 2012 Sep;19(5):1079-86. doi: 10.1016/j.ultsonch.2012.01.013. Epub 2012 Feb 4.
Mercury selenide (HgSe) nanostructures were synthesized via a sonochemical method based on the reaction between HgCl(2), SeCl(4) and hydrazine hydrate (N(2)H(4)·H(2)O) in water, in presence of various capping agents. The effects of preparation parameters such as: the kind of capping agent and its amount, ultrasonic power, reaction time and temperature were investigated. It was found that morphology, particle size and phase of the products could be greatly affected by these parameters. HgSe nanostructures were characterized by X-ray powder diffraction (XRD), transmission electron microscopy (TEM), scanning electron microscopy (SEM), photoluminescence spectroscopy (PL) and X-ray energy dispersive spectroscopy (EDS).
通过基于在水存在下 HgCl2、SeCl4 和水合肼（N2H4·H2O）之间的反应的超声化学方法，合成了硒化汞（HgSe）纳米结构，使用了各种封端剂。研究了诸如：封端剂的种类及其用量、超声功率、反应时间和温度等制备参数的影响。结果发现，这些参数可以极大地影响产物的形态、粒径和相。通过 X 射线粉末衍射（XRD）、透射电子显微镜（TEM）、扫描电子显微镜（SEM）、光致发光光谱（PL）和 X 射线能量色散光谱（EDS）对 HgSe 纳米结构进行了表征。
