Department of Dental and Biomedical Material Sciences, Graduate School of Biomedical Sciences, Nagasaki University, Nagasaki, Japan.
J Endod. 2012 Aug;38(8):1126-9. doi: 10.1016/j.joen.2012.04.013. Epub 2012 Jun 17.
Mineral trioxide aggregate (MTA) has been used successfully for perforation repair, vital pulpotomies, and direct pulp capping. However, little is known about the interactions between MTA and glass ionomer cement (GIC) in final restorations. In this study, 2 null hypotheses were tested: (1) GIC placement time does not affect the MTA-GIC structural interface and hardness and (2) moisture does not affect the MTA-GIC structural interface and hardness.
Fifty cylinders were half filled with MTA and divided into 5 groups. The other half was filled with resin-modified GIC either immediately after MTA placement or after 1 or 7 days of temporization in the presence or absence of a wet cotton pellet. The specimens were then sectioned, carbon coated, and examined using a scanning electron microscope and an electron probe microanalyzer (SEM-EPMA) for interfacial adaptation, gap formation, and elemental analysis. The Vickers hardness numbers of the interfacial MTA were recorded 24 hours after GIC placement and 8 days after MTA placement and analyzed using the analysis of variance test.
Hardness testing 24 hours after GIC placement revealed a significant increase in hardness with an increase of temporization time but not with a change of moisture conditions (P < .05). Hardness testing 8 days after MTA placement indicated no significant differences among groups. SEM-EPMA showed interfacial adaptation to improve with temporization time and moisture. Observed changes were limited to the outermost layer of MTA. The 2 null hypotheses were not rejected.
GIC can be applied over freshly mixed MTA with minimal effects on the MTA, which seemed to decrease with time.
矿物三氧化物聚合体(MTA)已成功用于穿孔修复、活髓切断和直接盖髓。然而,对于 MTA 和玻璃离子水门汀(GIC)在最终修复中的相互作用知之甚少。本研究检验了 2 个零假设:(1)GIC 放置时间不会影响 MTA-GIC 结构界面和硬度;(2)水分不会影响 MTA-GIC 结构界面和硬度。
将 50 个圆柱体的一半填充 MTA,并将其分为 5 组。另一半填充树脂改良型 GIC,分别在 MTA 放置后立即或在存在或不存在湿棉片的情况下放置 1 天或 7 天后填充。然后将标本切片、碳涂覆,并使用扫描电子显微镜和电子探针微分析仪(SEM-EPMA)检查界面适应性、间隙形成和元素分析。在 GIC 放置后 24 小时和 MTA 放置后 8 天记录界面 MTA 的维氏硬度值,并使用方差分析进行分析。
GIC 放置后 24 小时进行的硬度测试显示,随着暂封时间的增加,硬度显著增加,但水分条件的变化没有影响(P<0.05)。MTA 放置后 8 天的硬度测试表明,各组之间没有显著差异。SEM-EPMA 显示界面适应性随着暂封时间和水分的增加而提高。观察到的变化仅限于 MTA 的最外层。2 个零假设未被拒绝。
GIC 可涂覆在新鲜混合的 MTA 上,对 MTA 的影响最小,且似乎随着时间的推移而减小。