All India Network Project on Pesticide Residues, Directorate of Research, Bidhan Chandra Krishi Viswavidyalaya, Kalyani, Nadia, 741235, West Bengal, India.
Bull Environ Contam Toxicol. 2012 Sep;89(3):598-601. doi: 10.1007/s00128-012-0731-7. Epub 2012 Jul 15.
In order to examine the persistence behavior, safety evaluation and utilization of residue data for fixation of thiacloprid MRL, a supervised field trial in tea was conducted at Darjeeling. The HPLC analysis of thiacloprid in green tea leaves indicates that the initial deposits of 2.14 and 3.95 mg kg(-1), which declined gradually and persisted until day 14 to the tune of 0.23 and 0.45 mg kg(-1) respectively. The residues in processed tea samples prepared from green tea leaves of 7 and 14th day were 3.0-3.8 times less. Thiacloprid did not infuse to tea liquor from processed tea. The half-life value in green tea leaves ranged from 4.29 to 4.31 days. Considering the EU MRL value of 10 mg kg(-1) and risk assessment calculation, thiacloprid at 30 g a.i. ha(-1) appears to be safe in plant protection schedules and first round of plucking of green tea leaves on day 7 is recommended.
为了考察噻虫啉 MRL 的固定残留持久性、安全性评价和再利用,在大吉岭进行了一项茶树的有监管田间试验。高效液相色谱法分析表明,噻虫啉在绿茶叶片中的初始沉积量为 2.14 和 3.95mg/kg,逐渐下降,直至第 14 天分别降至 0.23 和 0.45mg/kg。由第 7 天和第 14 天的绿茶叶片制备的加工茶样品中的残留量分别减少了 3.0-3.8 倍。噻虫啉不会从加工茶中浸出到茶液中。噻虫啉在绿茶叶片中的半衰期值范围为 4.29 至 4.31 天。考虑到欧盟的 MRL 值为 10mg/kg 和风险评估计算,噻虫啉在 30g a.i./ha 的用量下,在植保计划中似乎是安全的,建议在第 7 天进行第一轮采摘。