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N-Acetyl-5-chloro-3-nitro-l-tyrosine ethyl ester.

作者信息

Mutahi Teresa T, Edagwa Benson J, Fronczek Frank R, Uppu Rao M

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2012 Sep 1;68(Pt 9):o2810-1. doi: 10.1107/S1600536812036380. Epub 2012 Aug 31.

Abstract

The title compound, C(13)H(15)ClN(2)O(6), was synthesized by hypochlorous acid-mediated chlorination of N-acetyl-3-nitro-l-tyrosine ethyl ester. The OH group forms an intra-molecular O-H⋯O hydrogen bond to the nitro group and the N-H group forms an inter-molecular N-H⋯O hydrogen bonds to an amide O atom, linking the mol-ecules into chains along [100]. The crystal studied was a non-merohedral twin, with a 0.907 (4):0.093 (4) domain ratio.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ad98/3435836/89eadebf45ae/e-68-o2810-fig1.jpg

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