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含不同光引发剂的实验性复合材料的颜色稳定性。

Color stability of experimental composites containing different photoinitiators.

机构信息

Department of Dental Materials and Prosthodontics, Ribeirão Preto School of Dentistry, University of São Paulo, Ribeirão Preto, SP, Brazil.

出版信息

J Dent. 2013 Aug;41 Suppl 3:e62-6. doi: 10.1016/j.jdent.2012.10.009. Epub 2012 Oct 23.

Abstract

OBJECTIVES

To evaluate the color stability (ΔE) of experimental composites containing different photoinitiators when submitted to accelerated artificial ageing (AAA).

MATERIAL AND METHODS

Thirty test specimens were made in a Teflon matrix (8mm×2mm), using an experimental composite (n=10) with the same monomer composition and particle size, but varying photoinitiator used: Group CQ (0.4% Camphorquinone), Group PPD (0.4% 1-Phenyl-1,2 Propanodione) and Group CQ+PPD (0.2% CQ+0.2% PPD). The samples were light activated (QTH - Ultralux - Dabi Atlante - 40s) and polished before performing the initial color readouts (EasyShade - Vita). Next, they were submitted to AAA for 300h, after which final color readouts were made.

RESULTS

The results (1-way ANOVA - Tukey - p<0.05) demonstrated that all the groups presented color alteration above the clinically acceptable level (ΔE≥3.3), however, with no statistically significant difference among them (p>0.05). Analysis of Δb demonstrated increase in the values of this coordinate, indicating yellowing in all groups.

CONCLUSIONS

It was concluded that the type of photoinitiator, which presented a tendency towards yellowing, did not interfere in the color stability of composites submitted to AAA.

CLINICAL SIGNIFICANCE

Alternative photoinitiators have been extensively studied since Camphorquinone presents a yellowish color, which compromises the aesthetic performance of composites, especially the lighter-shade ones.

摘要

目的

评估含有不同光引发剂的实验性复合材料在加速人工老化(AAA)下的颜色稳定性(ΔE)。

材料和方法

在聚四氟乙烯基质(8mm×2mm)中制作了 30 个测试样本,使用具有相同单体组成和粒径但使用不同光引发剂的实验性复合材料(n=10):CQ 组(0.4%樟脑醌)、PPD 组(0.4%1-苯基-1,2 丙二酮)和 CQ+PPD 组(0.2%CQ+0.2%PPD)。在进行初始颜色读数(EasyShade-Vita)之前,用光激活(QTH-Ultralux-Dabi Atlante-40s)和抛光样品。然后,将它们进行 AAA 300h,之后进行最终颜色读数。

结果

(单向方差分析- Tukey-p<0.05)结果表明,所有组的颜色变化均超过临床可接受水平(ΔE≥3.3),但它们之间无统计学差异(p>0.05)。Δb 的分析表明该坐标值增加,表明所有组均变黄。

结论

光引发剂的类型虽然有变黄的趋势,但不会影响 AAA 处理后的复合材料的颜色稳定性。

临床意义

由于樟脑醌呈黄色,会影响复合材料的美学性能,特别是浅色复合材料,因此已经广泛研究了替代光引发剂。

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