Bauru School of Dentistry, University of São Paulo, Bauru, SP, Brazil.
J Appl Oral Sci. 2012 Sep-Oct;20(5):556-62. doi: 10.1590/s1678-77572012000500011.
To determine the micro-hardness profile of two dual cure resin cements (RelyX-U100, 3M-eSPe and Panavia F 2.0, Kuraray) used for cementing fiberre inforced resin posts (Fibrekor-Jeneric Pentron) under three different curing protocols and two water storage times.
Sixty 16 mm long bovine incisor roots were endodontically treated and prepared for cementation of the Fibrekor posts. The cements were mixed as instructed, dispensed in the canal, the posts were seated and the curing performed as follows: (a) no light activation; (b) light-activation immediately after seating the post, and; (c) light-activation delayed 5 minutes after seating the post. The teeth were stored in water and retrieved for analysis after 7 days and 3 months. The roots were longitudinally sectioned and the microhardness was determined at the cervical, middle and apical regions along the cement line. The data was analyzed by the three-way ANOVA test (curing mode, storage time and thirds) for each cement. The Tukey test was used for the post-hoc analysis.
Light-activation resulted in a significant increase in the microhardness. This was more evident for the cervical region and for the Panavia cement. Storage in water for 3 months caused a reduction of the micro-hardness for both cements. The U100 cement showed less variation in the micro-hardness regardless of the curing protocol and storage time.
The micro-hardness of the cements was affected by the curing and storage variables and were material-dependent.
确定两种双固化树脂水门汀(RelyX-U100、3M-eSPe 和 Panavia F 2.0、Kuraray)在三种不同固化方案和两种储水时间下用于粘结纤维增强树脂桩(Fibrekor-Jeneric Pentron)的微观硬度分布。
60 个 16mm 长的牛切牙根管经过牙髓治疗并准备粘结 Fibrekor 桩。按照说明混合水门汀,将其放入根管中,然后将桩就位,并按照以下三种方式进行固化:(a)不进行光激活;(b)在桩就位后立即进行光激活;(c)在桩就位后延迟 5 分钟进行光激活。将牙齿储存在水中,在 7 天和 3 个月后取出进行分析。将根部分别沿粘结线从近中、中间和根尖进行纵向切割,并在相应区域测量微观硬度。使用三因素方差分析(固化模式、储存时间和三等分)对每种水门汀的数据进行分析。采用 Tukey 检验进行事后分析。
光激活显著提高了微观硬度。对于颈部区域和 Panavia 水门汀,这种影响更为明显。在水中储存 3 个月会导致两种水门汀的微观硬度降低。无论固化方案和储存时间如何,U100 水门汀的微观硬度变化都较小。
水门汀的微观硬度受到固化和储存变量的影响,并且具有材料依赖性。