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固化方式对牙科自粘树脂水门汀表面能及吸附/溶解性的影响

Influence of Curing Mode on the Surface Energy and Sorption/Solubility of Dental Self-Adhesive Resin Cements.

作者信息

Kim Hyun-Jin, Bagheri Rafat, Kim Young Kyung, Son Jun Sik, Kwon Tae-Yub

机构信息

Department of Dental Science, Graduate School, Kyungpook National University, Daegu 41940, Korea.

Dental Materials Department and Biomaterials Research Centre, Shiraz University of Medical Sciences, Shiraz 7183643111, Iran.

出版信息

Materials (Basel). 2017 Feb 4;10(2):129. doi: 10.3390/ma10020129.

DOI:10.3390/ma10020129
PMID:28772489
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC5459112/
Abstract

This study investigated the influence of curing mode (dual- or self-cure) on the surface energy and sorption/solubility of four self-adhesive resin cements (SARCs) and one conventional resin cement. The degree of conversion (DC) and surface energy parameters including degree of hydrophilicity (DH) were determined using Fourier transform infrared spectroscopy and contact angle measurements, respectively ( = 5). Sorption and solubility were assessed by mass gain or loss after storage in distilled water or lactic acid for 60 days ( = 5). A linear regression model was used to correlate between the results (%DC vs. DH and %DC/DH vs. sorption/solubility). For all materials, the dual-curing consistently produced significantly higher %DC values than the self-curing ( < 0.05). Significant negative linear regressions were established between the %DC and DH in both curing modes ( < 0.05). Overall, the SARCs showed higher sorption/solubility values, in particular when immersed in lactic acid, than the conventional resin cement. Linear regression revealed that %DC and DH were negatively and positively correlated with the sorption/solubility values, respectively. Dual-curing of SARCs seems to lower the sorption and/or solubility in comparison with self-curing by increased %DC and occasionally decreased hydrophilicity.

摘要

本研究调查了固化方式（双重固化或自固化）对四种自粘树脂水门汀（SARC）和一种传统树脂水门汀的表面能以及吸附/溶解性的影响。分别使用傅里叶变换红外光谱法和接触角测量法测定转化率（DC）和亲水性程度（DH）等表面能参数（n = 5）。通过在蒸馏水或乳酸中储存60天后的质量增加或减少来评估吸附和溶解性（n = 5）。使用线性回归模型来关联结果（%DC与DH以及%DC/DH与吸附/溶解性之间的关系）。对于所有材料，双重固化始终产生显著高于自固化的%DC值（P < 0.05）。在两种固化方式下，%DC与DH之间均建立了显著的负线性回归关系（P < 0.05）。总体而言，SARC显示出比传统树脂水门汀更高的吸附/溶解性值，尤其是在浸入乳酸中时。线性回归表明，%DC和DH分别与吸附/溶解性值呈负相关和正相关。与自固化相比，SARC的双重固化似乎通过提高%DC和偶尔降低亲水性来降低吸附和/或溶解性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/0ca7ee2271c5/materials-10-00129-g007a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/4905f8455b13/materials-10-00129-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/2fb165523216/materials-10-00129-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/eb0cfdbc895d/materials-10-00129-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/477d03aa852b/materials-10-00129-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/352688e47f94/materials-10-00129-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/143e5460be20/materials-10-00129-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/0ca7ee2271c5/materials-10-00129-g007a.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/4905f8455b13/materials-10-00129-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/2fb165523216/materials-10-00129-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/eb0cfdbc895d/materials-10-00129-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/477d03aa852b/materials-10-00129-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/352688e47f94/materials-10-00129-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/143e5460be20/materials-10-00129-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/8137/5459112/0ca7ee2271c5/materials-10-00129-g007a.jpg

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