Suppr超能文献

不同光固化方法对通过陶瓷片聚合的树脂水门汀机械和物理性能的影响。

Effect of different light curing methods on mechanical and physical properties of resin-cements polymerized through ceramic discs.

机构信息

Department of Prosthodontics, Faculty of Dentistry, Gazi University, Ankara, Turkey.

出版信息

J Appl Oral Sci. 2011 Aug;19(4):403-12. doi: 10.1590/s1678-77572011005000017. Epub 2011 Jul 1.

Abstract

OBJECTIVE

The aim of this study was to compare the polimerization ability of three different light-curing units (quartz tungsten halogen, light-emitting diodes and plasma arc) and their exposure modes (high-intensity and soft-start) by determination of microhardness, water sorption and solubility, and diametral tensile strength of 5 dual-curing resin cements.

MATERIAL AND METHODS

A total of 720 disc-shaped samples (1 mm height and 5 mm diameter) were prepared from different dual-curing resin cements (Duolink, Nexus, Bifix-QM, Panavia F and RelyX Unicem). Photoactivation was performed by using quartz tungsten halogen (high-power and soft-up modes), light-emitting diode (standard and exponential modes) and plasma arc (normal and ramp-curing modes) curing units through ceramic discs. Then the samples (n=8/per group) were stored dry in the dark at 37°C for 24 h. The Vickers hardness test was performed on the resin cement layer with a microhardness tester (Shimadzu HMV). For sorption and solubility tests; the samples were stored in a desiccator at 37°C and weighed to a constant mass. The samples were weighed both before and after being immersed in deionized water for different periods of time (24 h and 7 days) and being desiccated. The diametral tensile strength of the samples was tested in a universal testing machine at a crosshead speed of 0.5 mm/min. Data were analyzed statistically by nonparametric Kruskal Wallis and Mann-Whitney U tests at 5% significance level.

RESULTS

Resin cement and light-curing unit had significant effects (p<0.05) on microhardness, diametral tensile strength, water solubility and sorption. However, no significant differences (p>0.05) were obtained with different modes of LCUs.

CONCLUSION

The study indicates that polymerization of resin cements with different light-curing units may result in various polymer structures, and consequently different mechanical and physical properties.

摘要

目的

本研究旨在比较三种不同的光固化单元(石英钨卤素、发光二极管和等离子电弧)及其曝光模式(高强度和软启动)的聚合能力,通过测定 5 种双固化树脂水门汀的显微硬度、吸水和溶胀率以及直径拉伸强度来评估。

材料与方法

从不同的双固化树脂水门汀(Duolink、Nexus、Bifix-QM、Panavia F 和 RelyX Unicem)中制备了 720 个圆盘状样本(高度 1mm,直径 5mm)。通过陶瓷盘用光固化单元(高功率和软启动模式)、发光二极管(标准和指数模式)和等离子电弧(正常和斜坡固化模式)对样本进行光固化。然后将样本(n=8/组)在 37°C 下黑暗中干燥保存 24 小时。使用显微硬度计(Shimadzu HMV)对树脂水门汀层进行维氏硬度测试。为了进行吸水和溶胀测试,将样本储存在 37°C 的干燥器中,并在恒质量下称重。将样本在不同时间段(24 小时和 7 天)浸入去离子水中并干燥后,分别进行称重。使用万能试验机以 0.5mm/min 的十字头速度测试样本的直径拉伸强度。在 5%的显著性水平下,采用非参数 Kruskal Wallis 和 Mann-Whitney U 检验对数据进行统计分析。

结果

树脂水门汀和光固化单元对显微硬度、直径拉伸强度、水溶解度和吸水有显著影响(p<0.05)。然而,LCU 的不同模式之间没有得到显著差异(p>0.05)。

结论

研究表明,不同光固化单元聚合树脂水门汀可能导致不同的聚合结构,进而产生不同的机械和物理性能。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a6fd/4223794/c5b11b5bc453/jaos-19-04-0403-g01.jpg

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验