Adhesive Dentistry Research Group, Department of Cariology, Institute of Dentistry, University of Turku, Turku, Finland.
Dent Mater. 2013 Apr;29(4):437-49. doi: 10.1016/j.dental.2013.01.008. Epub 2013 Feb 21.
There are concerns regarding the longevity of resin composite restorations and the clinical relevance of in vitro bond strength testing to the durability of dentin bonds in vivo.
The objectives of this investigation were to: (1) develop a new method of experimental evaluation for quantifying the durability of dentin bonds, (2) apply this method to characterize the interfacial strength of a selected commercial system under both monotonic and cyclic loading, and (3) distinguish mechanisms contributing to the interface degradation and failure.
A new method for fatigue testing the resin-dentin interface was developed based on a four-point flexure arrangement that includes two identical bonded interfaces. Cyclic loading of specimens comprised of coronal dentin bonded to a commercial resin composite and controls of resin composite was performed to failure within a hydrated environment. Scanning electron microscopy and nanoscopic dynamic mechanical analysis were used to evaluate failure mechanisms.
The fatigue strength of the resin-dentin interface was significantly lower (p≤0.0001) than that of the resin composite and reported for dentin over the entire finite life regime. Defined at 1×10(7) cycles, the apparent endurance limit of the resin-dentin interface was 13MPa, in comparison to 48MPa and 44MPa for the resin composite and dentin, respectively. The ratio of fully reversed endurance limit to ultimate strength of the interface (0.26) was the lowest of the three materials.
The proposed approach for characterizing the fatigue strength of resin-dentin bonds may offer new insights concerning durability of the bonded interface.
人们对树脂复合材料修复体的耐久性以及体外粘结强度测试对牙本质粘结体内耐久性的临床相关性存在担忧。
本研究的目的是:(1)开发一种新的实验评估方法来量化牙本质粘结体的耐久性;(2)应用该方法来描述选定商业系统在单调和循环加载下的界面强度;(3)区分导致界面降解和失效的机制。
基于四点弯曲装置开发了一种新的用于疲劳测试树脂-牙本质界面的方法,该装置包括两个相同的粘结界面。在水合环境下对由冠部牙本质粘结到商业树脂复合材料的标本和复合材料对照进行循环加载直至失效。扫描电子显微镜和纳米动态力学分析用于评估失效机制。
树脂-牙本质界面的疲劳强度明显低于(p≤0.0001)树脂复合材料和整个有限寿命范围内的牙本质报道值。在 1×10(7)循环处定义的树脂-牙本质界面的表观疲劳极限为 13MPa,而树脂复合材料和牙本质的疲劳极限分别为 48MPa 和 44MPa。界面完全反转疲劳极限与极限强度的比值(0.26)是三种材料中最低的。
用于描述树脂-牙本质粘结体疲劳强度的方法可能为粘结界面的耐久性提供新的见解。