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双(4-{2-[4-(二乙氨基)-苯基]乙烯基}吡啶-κN)二碘锌

Bis(4-{2-[4-(diethyl-amino)-phen-yl]ethen-yl}pyridine-κN)diiodidozinc.

作者信息

Nie Cui-Yun, Tian Yu-Peng

机构信息

Department of Chemistry, Anhui University, Hefei 230039, People's Republic of China ; Key Laboratory of Functional Inorganic Materials, Chemistry, Hefei 230039, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 1;69(Pt 3):m135. doi: 10.1107/S1600536813001736. Epub 2013 Feb 2.

DOI:10.1107/S1600536813001736
PMID:23476485
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3588506/
Abstract

In the title compound, [ZnI2(C17H20N2)2], the Zn(II) atom is four-coordinated by two I atoms and the N atoms of two pyridine rings belonging to different ligands in a distorted tetra-hedral geometry. The coordinating pyridine rings are oriented in an almost perpendicular fashion, making a dihedral angle of 83.7 (5)°.

摘要

在标题化合物[ZnI₂(C₁₇H₂₀N₂)₂]中，Zn(II)原子由两个碘原子以及属于不同配体的两个吡啶环的氮原子以扭曲的四面体几何构型进行四配位。配位的吡啶环以几乎垂直的方式取向，二面角为83.7 (5)°。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a94a/3588506/bdbabb9e6991/e-69-0m135-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a94a/3588506/bdbabb9e6991/e-69-0m135-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/a94a/3588506/bdbabb9e6991/e-69-0m135-fig1.jpg

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本文引用的文献

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J Am Chem Soc. 2009 Apr 15;131(14):5208-13. doi: 10.1021/ja808606d.
2
A short history of SHELX.SHELX简史。
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.