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(E)-N'-(4-Fluoro-benzyl-idene)-2-(3-methyl-phen-yl)acetohydrazide.

作者信息

Praveen A S, Jasinski Jerry P, Keeley Amanda C, Yathirajan H S, Narayana B

机构信息

Department of Studies in Chemistry, University of Mysore, Manasagangotri, Mysore 570 006, India.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 1;69(Pt 3):o421. doi: 10.1107/S1600536813004467. Epub 2013 Feb 23.

DOI:10.1107/S1600536813004467
PMID:23476595
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC3588440/
Abstract

In the title compound, C16H15FN2O, the dihedral angles between the benzene rings are74.7(8), 74.1 (1), 74.2 (7) and 74.3 (5)° in the four independent mol-ecules in the asymmetric unit. In the crystal, N-H-O hydrogen bonds involving the hydrazide and acetyl groups, which form R2(2)(18) ring motifs, link the mol-ecules into dimers, which form columns along [010].

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1182/3588440/f5df4785d425/e-69-0o421-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1182/3588440/6ffdf2a74851/e-69-0o421-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1182/3588440/f5df4785d425/e-69-0o421-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1182/3588440/6ffdf2a74851/e-69-0o421-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1182/3588440/f5df4785d425/e-69-0o421-fig2.jpg

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3
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A short history of SHELX.SHELX简史。
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