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微制造的 1-3 复合材料声匹配层用于 15MHz 换能器。

Microfabricated 1-3 composite acoustic matching layers for 15 MHz transducers.

机构信息

Department of Micro and Nano Systems Technology, Vestfold University College, Horten, Norway.

出版信息

Ultrasonics. 2013 Aug;53(6):1141-9. doi: 10.1016/j.ultras.2013.02.010. Epub 2013 Mar 5.

Abstract

Medical ultrasound transducers require matching layers to couple energy from the piezoelectric ceramic into the tissue. Composites of type 0-3 are often used to obtain the desired acoustic impedances, but they introduce challenges at high frequencies, i.e. non-uniformity, attenuation, and dispersion. This paper presents novel acoustic matching layers made as silicon-polymer 1-3 composites, fabricated by deep reactive ion etch (DRIE). This fabrication method is well-established for high-volume production in the microtechnology industry. First estimates for the acoustic properties were found from the iso-strain theory, while the Finite Element Method (FEM) was employed for more accurate modeling. The composites were used as single matching layers in 15 MHz ultrasound transducers. Acoustic properties of the composite were estimated by fitting the electrical impedance measurements to the Mason model. Five composites were fabricated. All had period 16 μm, while the silicon width was varied to cover silicon volume fractions between 0.17 and 0.28. Silicon-on-Insulator (SOI) wafers were used to get a controlled etch stop against the buried oxide layer at a defined depth, resulting in composites with thickness 83 μm. A slight tapering of the silicon side walls was observed; their widths were 0.9 μm smaller at the bottom than at the top, corresponding to a tapering angle of 0.3°. Acoustic parameters estimated from electrical impedance measurements were lower than predicted from the iso-strain model, but fitted within 5% to FEM simulations. The deviation was explained by dispersion caused by the finite dimensions of the composite and by the tapered walls. Pulse-echo measurements on a transducer with silicon volume fraction 0.17 showed a two-way -6 dB relative bandwidth of 50%. The pulse-echo measurements agreed with predictions from the Mason model when using material parameter values estimated from electrical impedance measurements. The results show the feasibility of the fabrication method and the theoretical description. A next step would be to include these composites as one of several layers in an acoustic matching layer stack.

摘要

医学超声换能器需要匹配层将来自压电陶瓷的能量耦合到组织中。0-3 型复合材料通常用于获得所需的声阻抗,但在高频下会带来非均匀性、衰减和色散等挑战。本文提出了一种新颖的声学匹配层,由硅-聚合物 1-3 复合材料制成,采用深反应离子刻蚀(DRIE)制备。这种制造方法在微技术行业中已经得到了广泛应用,可以实现大规模生产。首先,根据等应变理论对声特性进行了初步估计,然后采用有限元法(FEM)进行更准确的建模。该复合材料被用作 15MHz 超声换能器中的单一匹配层。通过将电阻抗测量值拟合到 Mason 模型来估算复合材料的声学特性。共制备了 5 种复合材料。所有复合材料的周期均为 16μm,而硅的宽度不同,覆盖了 0.17 至 0.28 的硅体积分数。使用绝缘体上硅(SOI)晶片以在规定深度处获得对埋层氧化物层的可控刻蚀停止,从而得到厚度为 83μm 的复合材料。观察到硅侧壁略有锥形;底部比顶部窄 0.9μm,对应的锥角为 0.3°。从电阻抗测量中估算出的声学参数低于等应变模型的预测值,但与 FEM 模拟拟合在 5%以内。偏差是由复合材料的有限尺寸和锥形壁引起的色散引起的。在硅体积分数为 0.17 的换能器上进行的脉冲回波测量显示,双向-6dB 相对带宽为 50%。当使用从电阻抗测量中估算出的材料参数值时,Mason 模型的脉冲回波测量与预测值吻合较好。结果表明,该制造方法和理论描述具有可行性。下一步是将这些复合材料作为声学匹配层堆叠中的一层或多层之一。

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