5-Iodo-3-phenyl-2,1-benzoxazole.
作者信息
Teslenko Yuriy, Matiychuk Vasyl S, Kinzhybalo Vasyl, Lis Tadeusz, Obushak Mykola D
机构信息
Department of Organic Chemistry, Ivan Franko National University of Lviv, Kyryla and Mefodiya 6, Lviv 79005, Ukraine.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 9;69(Pt 4):o508. doi: 10.1107/S1600536813005862. Print 2013 Apr 1.
Abstract
The title compound, C13H8INO, was prepared by a condensation reaction of 4-nitro-benzene with phenyl-acetonitrile in NaOH-ethanol solution. There are two independent mol-ecules in the asymmetric unit, in which the dihedral angles between the benzene ring and the benzoisoxazole unit are 4.2 (3) and 4.1 (3)°. The crystal packing is governed by C-H⋯N, C-I⋯π and C-I⋯O inter-actions.
摘要
相似文献
1
5-Iodo-3-phenyl-2,1-benzoxazole.
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 9;69(Pt 4):o508. doi: 10.1107/S1600536813005862. Print 2013 Apr 1.
2
2-Iodo-N-(6-methyl-2-pyrid-yl)benzamide.
Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 13;65(Pt 1):o118-9. doi: 10.1107/S1600536808041950.
3
Crystal structures of three carbazole derivatives: 12-ethyl-7-phenyl-sulfonyl-7-benzofuro[2,3-]carbazole, (1), 2-(4,5-dimeth-oxy-2-nitro-phen-yl)-4-hy-droxy-9-phenyl-sulfonyl-9-carbazole-3-carbaldehyde, (2), and 12-phenyl-7-phenyl-sulfonyl-7-benzofuro[2,3-]carbazole, (3).
Acta Crystallogr E Crystallogr Commun. 2016 Nov 4;72(Pt 12):1744-1750. doi: 10.1107/S2056989016016819. eCollection 2016 Dec 1.
4
4-[(5-Hydr-oxy-3-methyl-1-phenyl-1H-pyrazol-4-yl)phenyl-meth-yl]-5-methyl-2-phenyl-1H-pyrazol-3(2H)-one ethanol hemisolvate.
Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 10;65(Pt 1):o66-7. doi: 10.1107/S1600536808039081.
5
5-Iodo-2,7-dimethyl-3-phenyl-sulfonyl-1-benzofuran.
Acta Crystallogr Sect E Struct Rep Online. 2008 Apr 30;64(Pt 5):o930. doi: 10.1107/S1600536808011240.
6
6-Chloro-9-(2-nitro-phenyl-sulfon-yl)-9H-purine.
Acta Crystallogr Sect E Struct Rep Online. 2011 Feb 23;67(Pt 3):o687. doi: 10.1107/S1600536811003102.
7
4-Cyclo-butyl-amino-3-nitro-benzoic acid.
Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 13;65(Pt 7):o1566-7. doi: 10.1107/S1600536809021412.
8
2-(2H-Indazol-2-yl)-1-phenyl-ethanone.
Acta Crystallogr Sect E Struct Rep Online. 2013 Feb 1;69(Pt 2):o184. doi: 10.1107/S1600536812051811. Epub 2013 Jan 4.
9
4-(2-Nitro-benz-yl)-3-phenyl-3,4-di-hydro-2H-1,4-benzoxazin-2-ol.
Acta Crystallogr Sect E Struct Rep Online. 2014 Jul 11;70(Pt 8):o863-4. doi: 10.1107/S1600536814015645. eCollection 2014 Aug 1.
10
(Z)-N-[2-(N'-Hy-droxy-carbamimido-yl)phen-yl]acetamide.
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 1;69(Pt 3):o370-1. doi: 10.1107/S1600536813003371. Epub 2013 Feb 9.
本文引用的文献
1
3-(4-Chloro-phen-yl)-2,1-benzisoxazole-5-carbonyl chloride.
Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 22;64(Pt 12):o2420. doi: 10.1107/S1600536808037872.
2
A short history of SHELX.
Acta Crystallogr A. 2008 Jan;64(Pt 1):112-22. doi: 10.1107/S0108767307043930. Epub 2007 Dec 21.
3
5-imidazolyl-quinolinones, -quinazolinones and -benzo-azepinones as farnesyltransferase inhibitors.
Bioorg Med Chem Lett. 2003 May 5;13(9):1543-7. doi: 10.1016/s0960-894x(03)00180-x.
4
7-trifluoromethoxy and 7-trifluoromethylthio derivatives of 1,4-benzodiazepines.
J Med Chem. 1968 Nov;11(6):1248-50. doi: 10.1021/jm00312a602.
5
1-(2-aminoethyl)-6-aryl-4H- [1,2,4]triazolo[4,3-a][1,4]benzodiazepines with diuretic and natriuretic activity.
J Med Chem. 1989 Jun;32(6):1157-63. doi: 10.1021/jm00126a003.
6
Antiinflammatory agents. 4. Syntheses and biological evaluation of potential prodrugs of 2-amino-3-benzoylbenzeneacetic acid and 2-amino-3-(4-chlorobenzoyl)benzeneacetic acid.
J Med Chem. 1990 Aug;33(8):2296-304. doi: 10.1021/jm00170a039.
Zotero 插件