Teslenko Yuriy, Matiychuk Vasyl S, Kinzhybalo Vasyl, Lis Tadeusz, Obushak Mykola D
Department of Organic Chemistry, Ivan Franko National University of Lviv, Kyryla and Mefodiya 6, Lviv 79005, Ukraine.
Acta Crystallogr Sect E Struct Rep Online. 2013 Mar 9;69(Pt 4):o508. doi: 10.1107/S1600536813005862. Print 2013 Apr 1.
The title compound, C13H8INO, was prepared by a condensation reaction of 4-nitro-benzene with phenyl-acetonitrile in NaOH-ethanol solution. There are two independent mol-ecules in the asymmetric unit, in which the dihedral angles between the benzene ring and the benzoisoxazole unit are 4.2 (3) and 4.1 (3)°. The crystal packing is governed by C-H⋯N, C-I⋯π and C-I⋯O inter-actions.
标题化合物C₁₃H₈INO是通过4-硝基苯与苯乙腈在氢氧化钠-乙醇溶液中发生缩合反应制备的。不对称单元中有两个独立的分子，其中苯环与苯并异恶唑单元之间的二面角分别为4.2（3）°和4.1（3）°。晶体堆积由C-H⋯N、C-I⋯π和C-I⋯O相互作用控制。
