Ni Gang, Yu De-Quan
Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, State Key Laboratory of Bioactive Substances and Functions of Natural Medicines, Beijing 100050, China.
Zhongguo Zhong Yao Za Zhi. 2013 Feb;38(4):569-73.
Fifteen compounds were isolated from the rhizomes of Acorus tatarinowii by means of various chromatographic techniques such as silica gel, ODS, Sephadex LH-20 and preparative HPLC, and their structures were elucidated as tatanone A (1), calamusenone (2), acoronene (3), 2-acetyloxyacoronene (4), acorenone (5), alpha-asarone (6), beta-asarone (7), 1,2-dimethoxy-4-(1'Z-propenyl) benzene (8), methyleugenol (9), asarylaldehyde (10), acoramone (11), gamma-asarone (12), 5-hydroxymethyl-2-furaldehyde (13), galgravin (14) and eudesmin (15) on the basis of spectroscopic data analysis. Compound 1 was a new compound, and compounds 3-5 were separated from Acorus species for the first time.
通过硅胶、ODS、葡聚糖凝胶LH - 20和制备型高效液相色谱等多种色谱技术,从石菖蒲根茎中分离出15种化合物,并基于光谱数据分析确定其结构为塔他酮A(1)、菖蒲烯酮(2)、菖蒲烯(3)、2 - 乙酰氧基菖蒲烯(4)、菖蒲酮(5)、α-细辛醚(6)、β-细辛醚(7)、1,2 - 二甲氧基 - 4 -(1'Z - 丙烯基)苯(8)、甲基丁香酚(9)、细辛醛(10)、菖蒲酮(11)、γ-细辛醚(12)、5 - 羟甲基 - 2 - 糠醛(13)、加尔格拉文(14)和欧细辛醚(15)。化合物1为新化合物,化合物3 - 5首次从菖蒲属植物中分离得到。