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热应用对玻璃离子水门汀力学性能的影响。

Effect of heat application on the mechanical behaviour of glass ionomer cements.

作者信息

Menne-Happ Ulrike, Ilie Nicoleta

机构信息

Department of Restorative Dentistry, Dental School of the Ludwig-Maximilians-University, Goethestr. 70, 80336, Munich, Germany.

出版信息

Clin Oral Investig. 2014;18(2):643-50. doi: 10.1007/s00784-013-1005-4. Epub 2013 Jun 6.

Abstract

OBJECTIVES

The aim of this study was to examine the long-term effect of heat on the mechanical behaviour of conventional highly viscous glass ionomer cements. Besides, the effect of storage time was evaluated.

MATERIALS AND METHODS

Five cements (ChemFil Rock, Riva Self Cure, Fuji IX GP Fast, Equia and Ketac Molar Aplicap) were evaluated using three different preparation methods: no heat application, application of heat by means of a LED curing unit for 20 and 60 s. Four hundred fifty bar-shaped specimens were produced, maintained in distilled water at 37 °C and tested after 1 week, 1 month and 3 months (n = 10). The Vickers hardness, indentation modulus and creep were measured. In addition, the amount and size of the glass fillers and voids were examined using a light and a scanning electron microscope.

RESULTS

Fuji IX GP Fast showed the highest Vickers hardness, Ketac Molar Aplicap showed the highest indentation modulus and the best value of creep was measured for Riva Self Cure. Vickers hardness, modulus of elasticity and creep resistance increased most for ChemFil Rock and Equia up to 1-month storage.

CONCLUSIONS

Heat application showed no effect on the mechanical behaviour of ChemFil Rock, Fuji IX GP Fast and Equia at all ageing time. The impact of storage duration was low.

CLINICAL RELEVANCE

Considering the measured mechanical properties, there is no need of using heat when restoring teeth with glass ionomer cements.

摘要

目的

本研究旨在探讨加热对传统高粘性玻璃离子水门汀力学性能的长期影响。此外,还评估了储存时间的影响。

材料与方法

使用三种不同的制备方法对五种水门汀(ChemFil Rock、Riva Self Cure、Fuji IX GP Fast、Equia和Ketac Molar Aplicap)进行评估:不加热、通过LED固化灯加热20秒和60秒。制备了450个条形试件,保存在37℃的蒸馏水中,并在1周、1个月和3个月后进行测试(n = 10)。测量维氏硬度、压痕模量和蠕变。此外,使用光学显微镜和扫描电子显微镜检查玻璃填料和孔隙的数量及尺寸。

结果

Fuji IX GP Fast显示出最高的维氏硬度,Ketac Molar Aplicap显示出最高的压痕模量,Riva Self Cure的蠕变值最佳。ChemFil Rock和Equia在储存1个月时,维氏硬度、弹性模量和抗蠕变性增加最多。

结论

在所有老化时间下,加热对ChemFil Rock、Fuji IX GP Fast和Equia的力学性能均无影响。储存时间的影响较小。

临床意义

考虑到所测量的力学性能,使用玻璃离子水门汀修复牙齿时无需加热。

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