University of Campinas, School of Mechanical Engineering, Rua Mendeleiev 200, 13083-860 Campinas, Brazil.
J Mech Behav Biomed Mater. 2013 Oct;26:98-108. doi: 10.1016/j.jmbbm.2013.05.011. Epub 2013 May 29.
Rapid prototyping allows titanium porous parts with mechanical properties close to that of bone tissue to be obtained. In this article, porous parts of the Ti-6Al-4V alloy with three levels of porosity were obtained by selective laser melting with two different energy inputs. Thermal treatments were performed to determine the influence of the microstructure on the mechanical properties. The porous parts were characterized by both optical and scanning electron microscopy. The effective modulus, yield and ultimate compressive strength were determined by compressive tests. The martensitic α' microstructure was observed in all of the as-processed parts. The struts resulting from the processing conditions investigated were thinner than those defined by CAD models, and consequently, larger pores and a higher experimental porosity were achieved. The use of the high-energy input parameters produced parts with higher oxygen and nitrogen content, their struts that were even thinner and contained a homogeneous porosity distribution. Greater mechanical properties for a given relative density were obtained using the high-energy input parameters. The as-quenched martensitic parts showed yield and ultimate compressive strengths similar to the as-processed parts, and these were greater than those observed for the fully annealed samples that had the lamellar microstructure of the equilibrium α+β phases. The effective modulus was not significantly influenced by the thermal treatments. A comparison between these results and those of porous parts with similar geometry obtained by selective electron beam melting shows that the use of a laser allows parts with higher mechanical properties for a given relative density to be obtained.
快速原型制造允许获得机械性能接近骨组织的钛多孔零件。本文通过使用两种不同能量输入的选择性激光熔化获得了具有三个孔隙率水平的 Ti-6Al-4V 合金的多孔零件。进行了热处理以确定微观结构对机械性能的影响。通过光学显微镜和扫描电子显微镜对多孔零件进行了表征。通过压缩试验确定了有效模量、屈服强度和极限抗压强度。在所有加工零件中都观察到马氏体 α' 微观结构。由所研究的加工条件产生的支柱比 CAD 模型定义的支柱更薄,因此实现了更大的孔和更高的实验孔隙率。使用高能输入参数生产的零件具有更高的氧和氮含量,其支柱更薄,并且具有均匀的孔隙率分布。使用高能输入参数可以获得给定相对密度更高的机械性能。淬火马氏体零件的屈服强度和极限抗压强度与加工零件相似,并且大于具有平衡 α+β 相层状微观结构的完全退火样品的观察值。有效模量不受热处理的显著影响。对这些结果与通过选择性电子束熔化获得的具有相似几何形状的多孔零件的结果进行比较表明,激光的使用允许在给定相对密度下获得具有更高机械性能的零件。