Fischer M, Joguet D, Robin G, Peltier L, Laheurte P
Laboratoire d'Etude des Microstructures et de Mécanique des Matériaux LEM3 (UMR CNRS 7239), Université de Lorraine, Ile de Saulcy, F-57045 Metz, France.
Laboratoire d'Etudes et de Recherches sur les Matériaux, les Procédés et les Surfaces LERMPS, Université de Technologie de Belfort Montbéliard, Sevenans, 90010 Belfort, France.
Mater Sci Eng C Mater Biol Appl. 2016 May;62:852-9. doi: 10.1016/j.msec.2016.02.033. Epub 2016 Feb 11.
Ti-Nb alloys are excellent candidates for biomedical applications such as implantology and joint replacement because of their very low elastic modulus, their excellent biocompatibility and their high strength. A low elastic modulus, close to that of the cortical bone minimizes the stress shielding effect that appears subsequent to the insertion of an implant. The objective of this study is to investigate the microstructural and mechanical properties of a Ti-Nb alloy elaborated by selective laser melting on powder bed of a mixture of Ti and Nb elemental powders (26 at.%). The influence of operating parameters on porosity of manufactured samples and on efficacy of dissolving Nb particles in Ti was studied. The results obtained by optical microscopy, SEM analysis and X-ray microtomography show that the laser energy has a significant effect on the compactness and homogeneity of the manufactured parts. Homogeneous and compact samples were obtained for high energy levels. Microstructure of these samples has been further characterized. Their mechanical properties were assessed by ultrasonic measures and the Young's modulus found is close to that of classically elaborated Ti-26 Nbingot.
钛铌合金因其极低的弹性模量、优异的生物相容性和高强度,是植入学和关节置换等生物医学应用的理想候选材料。低弹性模量接近皮质骨,可将植入物插入后出现的应力屏蔽效应降至最低。本研究的目的是研究通过选择性激光熔化在钛和铌元素粉末(26原子%)混合物的粉末床上制备的钛铌合金的微观结构和力学性能。研究了操作参数对制造样品孔隙率以及铌颗粒在钛中溶解效果的影响。通过光学显微镜、扫描电子显微镜分析和X射线显微断层扫描获得的结果表明,激光能量对制造部件的致密性和均匀性有显著影响。在高能级下获得了均匀且致密的样品。对这些样品的微观结构进行了进一步表征。通过超声测量评估了它们的力学性能,发现杨氏模量接近传统制备的Ti-26Nb铸锭。