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纠错原子力显微镜:一种简单且广泛适用的方法,可显著提高原子力显微镜图像的准确性。

Error-corrected AFM: a simple and broadly applicable approach for substantially improving AFM image accuracy.

机构信息

University of Connecticut, Institute of Materials Science, Storrs, CT, USA.

出版信息

Nanotechnology. 2014 Apr 18;25(15):155704. doi: 10.1088/0957-4484/25/15/155704. Epub 2014 Mar 20.

Abstract

Atomic force microscopy (AFM) has become an indispensable tool for imaging the topography and properties of surfaces at the nanoscale. A ubiquitous problem, however, is that optimal accuracy demands smooth surfaces, slow scanning, and expert users, contrary to many AFM applications and practical use patterns. Accordingly, a simple correction to AFM topographic images is implemented, incorporating error signals such as deflection and/or amplitude data that have long been available but quantitatively underexploited. This is demonstrated to substantially improve both height and lateral accuracy for expert users, with a corresponding 3-5 fold decrease in image error. Common image artifacts due to inexperienced AFM use, generally poorly scanned surfaces, or high speed images acquired in as fast as 7 s, are also shown to be effectively rectified, returning results equivalent to standard 'expert-user' images. This concept is proven for contact mode AFM, AC-mode, and high speed imaging, as well as property mapping such as phase contrast, with obvious extensions to many specialized AFM variations as well. Conveniently, as this correction procedure is based on either real time or post-processing, it is easily employed for future as well as legacy AFM systems and data. Such error-corrected AFM therefore offers a simple, broadly applicable approach for more accurate, more efficient, and more user-friendly implementation of AFM for nanoscale topography and property mapping.

摘要

原子力显微镜(AFM)已成为在纳米尺度上成像表面形貌和特性的不可或缺的工具。然而,一个普遍存在的问题是,最优的准确性要求表面光滑、扫描缓慢且需要专家用户,这与许多 AFM 应用和实际使用模式相悖。因此,我们对 AFM 形貌图像进行了简单的校正,纳入了长期以来可用但定量利用不足的误差信号,例如偏转和/或振幅数据。这被证明可以显著提高专家用户的高度和横向精度,同时图像误差相应降低 3-5 倍。对于经验不足的 AFM 用户、通常扫描质量较差的表面或以最快 7 秒获取的高速图像等常见图像伪影,也可以有效地进行校正,返回与标准“专家用户”图像等效的结果。该概念已通过接触模式 AFM、AC 模式和高速成像以及相位对比度等特性映射得到验证,并且可以明显扩展到许多专门的 AFM 变体。方便的是,由于此校正过程基于实时或后处理,因此可以轻松用于未来和传统的 AFM 系统和数据。因此,经过误差校正的 AFM 为纳米级形貌和特性映射的 AFM 提供了一种简单、广泛适用的更准确、更高效、更用户友好的实现方法。

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