a Faculty of Science, Chemistry Department , University of Khartoum , Khartoum , Sudan.
Food Addit Contam Part B Surveill. 2014;7(2):135-40. doi: 10.1080/19393210.2013.859741. Epub 2014 Jan 8.
This survey examined 60 samples of sorghum and 30 samples of sorghum products from three states (Khartoum, Kordofan and Gadarif) of Sudan for aflatoxin B1, B2, G1 and G2 (AFB1, AFB2, AFG1, AFG2), ochratoxin A and B (OTA, OTB) and zearalenone (ZEN), using high performance liquid chromatography with fluorescence detection. The limits of detection and limits of quantification were in the range 0.01-0.6 µg kg(-1) and 0.03-2.0 µg kg(-1), respectively. The frequency of contaminated samples with AFB1 from Khartoum, Gadarif and Kordofan state was 38.1%, 22.2% and 23.8%, respectively. Only two samples of sorghum from Khartoum state were contaminated with OTA (3.3%). Concentrations of OTA and OTB were low and may not cause problems. No sample of sorghum or sorghum products was contaminated with ZEN. Some sorghum samples contained AFB1 concentrations above the European Union regulatory limits. The highest contaminated samples were found in Khartoum state.
本调查研究了苏丹三个州(喀土穆、科尔多凡和加达里夫)的 60 份高粱样本和 30 份高粱制品样本,采用高效液相色谱法和荧光检测法检测黄曲霉毒素 B1、B2、G1 和 G2(AFB1、AFB2、AFG1、AFG2)、赭曲霉毒素 A 和 B(OTA、OTB)和玉米赤霉烯酮(ZEN)。检测限和定量限分别在 0.01-0.6 µg kg(-1) 和 0.03-2.0 µg kg(-1) 范围内。来自喀土穆、加达里夫和科尔多凡州的 AFB1 污染样本的频率分别为 38.1%、22.2%和 23.8%。只有来自喀土穆州的两份高粱样本受到 OTA(3.3%)污染。OTA 和 OTB 的浓度较低,可能不会造成问题。没有高粱或高粱制品样本受到 ZEN 污染。一些高粱样本的 AFB1 浓度超过了欧盟监管限制。污染最严重的样本来自喀土穆州。