Çınar Serkan, Kırmalı Ömer
Department of Prosthodontics, Faculty of Dentistry, Akdeniz University, Antalya, Turkey.
J Adv Prosthodont. 2019 Oct;11(5):297-304. doi: 10.4047/jap.2019.11.5.297. Epub 2019 Oct 30.
This study investigated the repair bond strength of the zirconia ceramic after different aging conditions.
In order to imitate the failure modes of veneered zirconia restorations, veneer ceramic, zirconia, and veneer ceramic-zirconia specimens were prepared and were divided into 4 subgroups as: control (37℃ distilled water for 24 hours ) and 3000, 6000, 12000 thermal cycling groups (n=15). Then, specimens were bonded to composite resin using a porcelain repair kit according to the manufacturer recommendation. The repair bond strength (RBS) test was performed using a universal testing machine (0.5 mm/min). Failure types were analyzed under a stereomicroscope. Two-way ANOVA and Bonferroni test were used for statistical analysis.
The RBS values of zirconia specimens were statistically significant and higher than veneer ceramic and veneer ceramic-zirconia specimens in control, 3000 and 6000 thermal cycling groups (<.05). When 12000 thermal cycles were applied, the highest value was found in zirconia specimens but there was no statistically significant difference between veneer ceramic and veneer ceramic-zirconia specimens (>.05). Veneer ceramic specimens exhibited cohesive failure types, zirconia specimens exhibited adhesive failure types, and veneer ceramic-zirconia specimens exhibited predominately mixed failure types.
Thermal cycling can adversely affect RBS of composite resin bınded to level of fractured zirconia ceramics.
本研究调查了不同老化条件下氧化锆陶瓷的修复粘结强度。
为模拟贴面氧化锆修复体的失效模式,制备了贴面陶瓷、氧化锆以及贴面陶瓷 - 氧化锆试件,并分为4个亚组:对照组(37℃蒸馏水浸泡24小时)和3000、6000、12000次热循环组(n = 15)。然后,根据制造商的建议,使用瓷修复套件将试件粘结到复合树脂上。使用万能试验机(0.5 mm/min)进行修复粘结强度(RBS)测试。在立体显微镜下分析失效类型。采用双向方差分析和Bonferroni检验进行统计分析。
在对照组、3000次和6000次热循环组中,氧化锆试件的RBS值具有统计学意义且高于贴面陶瓷和贴面陶瓷 - 氧化锆试件(P <.05)。当进行12000次热循环时,氧化锆试件的RBS值最高,但贴面陶瓷和贴面陶瓷 - 氧化锆试件之间无统计学显著差异(P >.05)。贴面陶瓷试件表现为内聚破坏类型,氧化锆试件表现为粘结破坏类型,贴面陶瓷 - 氧化锆试件主要表现为混合破坏类型。
热循环会对粘结到断裂氧化锆陶瓷水平的复合树脂的RBS产生不利影响。