College of Light Industry and Food Engineering, Guangxi University, Nanning 530004, PR China.
College of Light Industry and Food Engineering, Guangxi University, Nanning 530004, PR China; Department of Chemical Engineering, University of New Brunswick, Fredericton, NB E3B5A3, Canada.
Bioresour Technol. 2015 Jun;185:21-7. doi: 10.1016/j.biortech.2015.02.052. Epub 2015 Feb 19.
To reduce the degradation of cellulose and obtain high molecular weight of hemicellulose from the extracts, pH pre-corrected hot water pretreatment was developed by employing sodium hydroxide (3.9mol/L). The response surface model was established to optimize the extraction process. The species composition and purity of hemicellulose extract was analyzed by High Performance Liquid Chromatography (HPLC). The obtained solid remainder was analyzed by FTIR and SEM. The results showed that the component of xylose in hemicellulose extract was similar with commercial xylan. FTIR and SEM were shown to be able to evaluate solid remainder composition and surface characterization of the bagasse. The biggest balance between solid remainder and dissolved solid was obtained. Not only the yield of dissolved solid was improved, but the structure of solid remainder was also proved, which was beneficial to pulping and papermaking.
为了降低纤维素的降解并从提取物中获得高分子量的半纤维素,采用氢氧化钠(3.9mol/L)开发了 pH 预先校正的热水预处理。建立响应面模型以优化提取工艺。通过高效液相色谱法(HPLC)对半纤维素提取物的种类组成和纯度进行分析。通过 FTIR 和 SEM 分析获得的固体残余物。结果表明,半纤维素提取物中木糖的成分与商业木聚糖相似。FTIR 和 SEM 被证明能够评估蔗渣的固体残余物组成和表面特性。获得了固体残余物和溶解固体之间的最佳平衡。不仅提高了溶解固体的产率,而且还证明了固体残余物的结构有利于制浆和造纸。