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温度、固化时间和填料组成对复合树脂表面显微硬度的影响。

Effect of temperature, curing time, and filler composition on surface microhardness of composite resins.

作者信息

Dionysopoulos Dimitrios, Papadopoulos Constantinos, Koliniotou-Koumpia Eugenia

机构信息

Department of Operative Dentistry, School of Dentistry, Aristotle University of Thessaloniki, Thessaloniki, Greece.

出版信息

J Conserv Dent. 2015 Mar-Apr;18(2):114-8. doi: 10.4103/0972-0707.153071.

Abstract

AIM

The aim of this study was to evaluate the microhardness of two composite resins when subjected to three different temperatures and three different light-curing times.

MATERIALS AND METHODS

Two composites were used; Filtek Z250 and Grandio. Three different temperatures (23, 37, and 55(o)C) were used, utilizing a composite warmer. The heated samples were immediately injected into cylindrical molds (6 mm × 2 mm) and the top surface of the specimens was polymerized for 10, 20, and 40 sec, using a Quartz-Tungsten-Halogen light-curing unit (QTH LCU). Vickers microhardness measurements were performed from both the top and bottom surface of the specimens, following dry storage for 24 hours in the dark. Statistical analysis were performed using one-way analysis of variance (ANOVA) and Tukey post-hoc test at a level of significance of a = 0.05.

RESULTS

The results indicated that there was an increase in microhardness as the temperature of the composite was increased for either the top or the bottom surface (P < 0.05). Furthermore, there was a general increase in microhardness for both composites as curing time increased (P < 0.05). The type of composites did not influence the surface microhardness (P > 0.05).

CONCLUSIONS

Temperature of composites affects their surface microhardness. Also, light-curing time influence microhardness values of the composites tested.

摘要

目的

本研究的目的是评估两种复合树脂在三种不同温度和三种不同光固化时间下的显微硬度。

材料与方法

使用了两种复合材料;Filtek Z250和Grandio。利用复合加热器采用三种不同温度(23、37和55(°C))。将加热后的样品立即注入圆柱形模具(6毫米×2毫米)中,并使用石英 - 钨 - 卤素光固化单元(QTH LCU)对样品的顶面进行10、20和40秒的聚合。在黑暗中干燥储存24小时后,从样品的顶面和底面进行维氏显微硬度测量。使用单因素方差分析(ANOVA)和Tukey事后检验进行统计分析,显著性水平为α = 0.05。

结果

结果表明,对于顶面或底面,随着复合材料温度的升高,显微硬度增加(P < 0.05)。此外,随着固化时间的增加,两种复合材料的显微硬度总体上都有所增加(P < 0.05)。复合材料的类型不影响表面显微硬度(P > 0.05)。

结论

复合材料的温度会影响其表面显微硬度。此外,光固化时间会影响所测试复合材料的显微硬度值。

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