• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

使用原位和在位 X 射线和中子散射进行功能材料分析。

Functional materials analysis using in situ and in operando X-ray and neutron scattering.

机构信息

Australian Nuclear Science and Technology Organisation, Locked Bag 2001, Kirrawee DC, New South Wales 2232, Australia.

Physik-Department, Fachgebiet Physik weicher Materie, Technische Universität München, James-Franck-Straße 1, 85748 Garching, Germany.

出版信息

IUCrJ. 2015 Feb 3;2(Pt 2):292-304. doi: 10.1107/S2052252514026062. eCollection 2015 Mar 1.

DOI:10.1107/S2052252514026062
PMID:25866665
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC4392421/
Abstract

In situ and in operando studies are commonplace and necessary in functional materials research. This review highlights recent developments in the analysis of functional materials using state-of-the-art in situ and in operando X-ray and neutron scattering and analysis. Examples are given covering a number of important materials areas, alongside a description of the types of information that can be obtained and the experimental setups used to acquire them.

摘要

原位和操作条件研究在功能材料研究中很常见且必要。本综述重点介绍了使用最先进的原位和操作条件 X 射线和中子散射及分析技术对功能材料进行分析的最新进展。给出了一些重要材料领域的实例,以及可以获得的信息类型和用于获取这些信息的实验设置的描述。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/c87d7c63d96d/m-02-00292-fig10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/7377fe244511/m-02-00292-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/9edae5d57a28/m-02-00292-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/8a2f8296ec86/m-02-00292-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/af51d94b8de0/m-02-00292-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/7c3bf2e4b346/m-02-00292-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/3edfcca51af4/m-02-00292-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/297d951b173e/m-02-00292-fig7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/608e1b75ba4d/m-02-00292-fig8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/e000e442e4c3/m-02-00292-fig9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/c87d7c63d96d/m-02-00292-fig10.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/7377fe244511/m-02-00292-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/9edae5d57a28/m-02-00292-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/8a2f8296ec86/m-02-00292-fig3.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/af51d94b8de0/m-02-00292-fig4.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/7c3bf2e4b346/m-02-00292-fig5.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/3edfcca51af4/m-02-00292-fig6.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/297d951b173e/m-02-00292-fig7.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/608e1b75ba4d/m-02-00292-fig8.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/e000e442e4c3/m-02-00292-fig9.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/1e7d/4392421/c87d7c63d96d/m-02-00292-fig10.jpg

相似文献

1
Functional materials analysis using in situ and in operando X-ray and neutron scattering.使用原位和在位 X 射线和中子散射进行功能材料分析。
IUCrJ. 2015 Feb 3;2(Pt 2):292-304. doi: 10.1107/S2052252514026062. eCollection 2015 Mar 1.
2
In Operando Neutron Scattering Multiple-Scale Studies of Lithium-Ion Batteries.锂离子电池的原位中子散射多尺度研究
Small. 2022 May;18(19):e2107491. doi: 10.1002/smll.202107491. Epub 2022 Feb 23.
3
Electrochemistry of Thin Films with In Situ/Operando Grazing Incidence X-Ray Scattering: Bypassing Electrolyte Scattering for High Fidelity Time Resolved Studies.采用原位/操作条件下掠入射X射线散射研究薄膜的电化学:绕过电解质散射以进行高保真时间分辨研究。
Small. 2021 Oct;17(42):e2103213. doi: 10.1002/smll.202103213. Epub 2021 Sep 21.
4
Review of Recent Development of In Situ/Operando Characterization Techniques for Lithium Battery Research.锂电池研究中原位/工况表征技术的最新进展综述
Adv Mater. 2019 Jul;31(28):e1806620. doi: 10.1002/adma.201806620. Epub 2019 May 17.
5
In Situ/Operando X-ray Spectroscopies for Advanced Investigation of Energy Materials.原位/操作态 X 射线光谱学在能源材料先进研究中的应用。
Chemistry. 2018 Dec 10;24(69):18356-18373. doi: 10.1002/chem.201803936. Epub 2018 Nov 15.
6
Proceedings of the International Workshop on Current Challenges in Liquid and Glass Science, (The Cosener's House, Abingdon 10-12 January 2007).《液体与玻璃科学当前挑战国际研讨会论文集》(2007年1月10日至12日于阿宾登科森纳之家)
J Phys Condens Matter. 2007 Oct 17;19(41):410301. doi: 10.1088/0953-8984/19/41/410301.
7
Probing morphology and chemistry in complex soft materials withresonant soft x-ray scattering.利用共振软X射线散射探测复杂软材料的形态和化学性质。
J Phys Condens Matter. 2021 Jun 17;33(31). doi: 10.1088/1361-648X/ac0194.
8
In Situ X-Ray Techniques for Electrochemical Interfaces.原位 X 射线技术在电化学界面中的应用。
Annu Rev Anal Chem (Palo Alto Calif). 2021 Jul 27;14(1):87-107. doi: 10.1146/annurev-anchem-091020-100631.
9
Li-ion half-cells studied during cycling by small-angle neutron scattering.通过小角中子散射研究循环过程中的锂离子半电池。
J Appl Crystallogr. 2020 Feb 1;53(Pt 1):210-221. doi: 10.1107/S160057671901714X.
10
Selected advances in small-angle scattering and applications they serve in manufacturing, energy and climate change.小角散射的选定进展及其在制造、能源和气候变化领域的应用。
J Appl Crystallogr. 2023 May 29;56(Pt 3):787-800. doi: 10.1107/S1600576723003898. eCollection 2023 Jun 1.

引用本文的文献

1
Operando Study Insights into Lithiation/Delithiation Processes in a Poly(ethylene oxide) Electrolyte of All-Solid-State Lithium Batteries by Grazing-Incidence X-ray Scattering.通过掠入射X射线散射对全固态锂电池聚环氧乙烷电解质中锂化/脱锂过程的原位研究洞察
ACS Appl Mater Interfaces. 2024 Jul 3;16(26):33307-33315. doi: 10.1021/acsami.4c01661. Epub 2024 Jun 24.
2
neutron diffraction to investigate the solid-state synthesis of Ni-rich cathode materials.利用中子衍射研究富镍正极材料的固态合成。
J Appl Crystallogr. 2023 Jun 23;56(Pt 4):1066-1075. doi: 10.1107/S1600576723004909. eCollection 2023 Aug 1.
3

本文引用的文献

1
Use of intermediate focus for grazing incidence small and wide angle x-ray scattering experiments at the beamline P03 of PETRA III, DESY.在德国电子同步加速器研究所(DESY)的佩特拉三号(PETRA III)光束线P03上,将中间焦点用于掠入射小角和广角X射线散射实验。
Rev Sci Instrum. 2014 Apr;85(4):043901. doi: 10.1063/1.4869784.
2
An in situ grazing incidence X-ray scattering study of block copolymer thin films during solvent vapor annealing.原位掠入射 X 射线散射研究嵌段共聚物薄膜在溶剂蒸气退火过程中的行为。
Adv Mater. 2014 Jan 15;26(2):273-81. doi: 10.1002/adma.201302562. Epub 2013 Nov 27.
3
Design of a humidity controlled sample stage for simultaneous conductivity and synchrotron X-ray scattering measurements.
Reaction dynamics studied femtosecond X-ray liquidography at X-ray free-electron lasers.
反应动力学研究了X射线自由电子激光下的飞秒X射线液体成像技术。
Chem Sci. 2022 Jun 6;13(29):8457-8490. doi: 10.1039/d2sc00502f. eCollection 2022 Jul 29.
4
Green Synthesis of Silver Nanoparticles Using the Flower Extract of for Cytotoxicity and Antimicrobial Studies.利用 花提取物的绿色合成法制备银纳米粒子及其细胞毒性和抗菌研究。
Int J Nanomedicine. 2021 May 14;16:3343-3356. doi: 10.2147/IJN.S307676. eCollection 2021.
5
Does crystallography need a new name?晶体学需要一个新名称吗?
IUCrJ. 2017 Jun 29;4(Pt 4):301-302. doi: 10.1107/S2052252517009484. eCollection 2017 Jul 1.
用于同时进行电导率和同步加速器X射线散射测量的湿度控制样品台的设计。
Rev Sci Instrum. 2013 Jul;84(7):075114. doi: 10.1063/1.4815981.
4
Cobalt nanoparticles growth on a block copolymer thin film: a time-resolved GISAXS study.钴纳米颗粒在嵌段共聚物薄膜上的生长:时间分辨 GISAXS 研究。
Langmuir. 2013 May 28;29(21):6331-40. doi: 10.1021/la400741b. Epub 2013 May 16.
5
From atoms to layers: in situ gold cluster growth kinetics during sputter deposition.从原子到层:溅射沉积过程中纳米金簇的原位生长动力学。
Nanoscale. 2013 Jun 7;5(11):5053-62. doi: 10.1039/c3nr34216f. Epub 2013 May 2.
6
In situ X-ray study of the structural evolution of gold nano-domains by spray deposition on thin conductive P3HT films.喷雾沉积在薄导电 P3HT 薄膜上的金纳米畴结构演变的原位 X 射线研究。
Langmuir. 2013 Feb 26;29(8):2490-7. doi: 10.1021/la3048483. Epub 2013 Feb 11.
7
Note: grazing incidence small and wide angle x-ray scattering combined with imaging ellipsometry.注意:掠入射小角与广角X射线散射结合成像椭偏仪。
Rev Sci Instrum. 2012 Jul;83(7):076107. doi: 10.1063/1.4738880.
8
Reversible Kirkwood-Alder transition observed in Pt3Cu2 nanoctahedron assemblies under controlled solvent annealing/drying conditions.在受控溶剂退火/干燥条件下观察到 Pt3Cu2 纳米八面体组装体中的可逆 Kirkwood-Alder 转变。
J Am Chem Soc. 2012 Aug 29;134(34):14043-9. doi: 10.1021/ja304108n. Epub 2012 Aug 17.
9
P03, the microfocus and nanofocus X-ray scattering (MiNaXS) beamline of the PETRA III storage ring: the microfocus endstation.P03,PETRA III 储存环的微聚焦和纳米聚焦 X 射线散射(MiNaXS)光束线:微聚焦端站。
J Synchrotron Radiat. 2012 Jul;19(Pt 4):647-53. doi: 10.1107/S0909049512016895. Epub 2012 May 10.
10
Phase separation in semidilute aqueous poly(N-isopropylacrylamide) solutions.半浓水溶液中聚 N-异丙基丙烯酰胺的相分离。
Langmuir. 2012 Jun 12;28(23):8791-8. doi: 10.1021/la3015332. Epub 2012 May 31.