†School of Physical Sciences - Chemistry and ‡Australian Centre for Research on Separation Science (ACROSS), University of Tasmania, Hobart, Tasmania 7001, Australia.
Org Lett. 2015 May 15;17(10):2428-30. doi: 10.1021/acs.orglett.5b00936. Epub 2015 May 4.
A new, practical, rapid, and high-yielding process for the pressurized hot water extraction (PHWE) of multigram quantities of shikimic acid from star anise (Illicium verum) using an unmodified household espresso machine has been developed. This operationally simple and inexpensive method enables the efficient and straightforward isolation of shikimic acid and the facile preparation of a range of its synthetic derivatives.
一种新的、实用的、快速的、高产的加压热水提取(PHWE)方法,可从八角(Illicium verum)中提取多克数量的莽草酸,使用未改装的家用浓缩咖啡机。这种操作简单且廉价的方法可有效且直接地分离莽草酸,并轻松制备其一系列合成衍生物。